N,N'-1,2-Ethanediylbis[3,5-bis(1,1-dimethylethyl)-4-hydroxybenzenepropanamide]

Base Information

Chemical Name:N,N'-1,2-Ethanediylbis[3,5-bis(1,1-dimethylethyl)-4-hydroxybenzenepropanamide]
CAS No.:23128-75-8
Molecular Formula:C₃₆H₅₆N₂O₄
Molecular Weight:580.852
Hs Code.:
DSSTox Substance ID:DTXSID701137368

Synonyms:N,N'-1,2-Ethanediylbis[3,5-bis(1,1-dimethylethyl)-4-hydroxybenzenepropanamide];23128-75-8;SCHEMBL1149914;DTXSID701137368;N,N'-1,2-ETHANEDIYL-BIS[3,5-BIS(1,1-DIMETHYLETHYL)-4-HYDROXYBENZENEPROPANAMIDE]

Suppliers and Price of N,N'-1,2-Ethanediylbis[3,5-bis(1,1-dimethylethyl)-4-hydroxybenzenepropanamide]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-1,2-Ethanediylbis[3,5-bis(1,1-dimethylethyl)-4-hydroxybenzenepropanamide]

Chemical Property:

XLogP3:8.6
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:13
Exact Mass:580.42400827
Heavy Atom Count:42
Complexity:753

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)C1=CC(=CC(=C1O)C(C)(C)C)CCC(=O)NCCNC(=O)CCC2=CC(=C(C(=C2)C(C)(C)C)O)C(C)(C)C

Technology Process of N,N'-1,2-Ethanediylbis[3,5-bis(1,1-dimethylethyl)-4-hydroxybenzenepropanamide]

There total 4 articles about N,N'-1,2-Ethanediylbis[3,5-bis(1,1-dimethylethyl)-4-hydroxybenzenepropanamide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.3%

: 64604-91-7
N-(2-aminoethyl)-3-[3,5-bis(tert-butyl)-4-hydroxyphenyl]propanamide

: 20170-32-5,90804-34-5
4-hydroxy-3,5-di-tert-butylphenylpropionic acid

: 23128-75-8
3-(3,5-Di-tert-butyl-4-hydroxy-phenyl)-N-{2-[3-(3,5-di-tert-butyl-4-hydroxy-phenyl)-propionylamino]-ethyl}-propionamide

Guidance literature:: With pyrographite; In 5,5-dimethyl-1,3-cyclohexadiene; at 140 ℃; for 10h; Inert atmosphere;

Reference yield:

: 107-15-3,85404-18-8
ethylenediamine

: 3062-64-4
3-(3,5-di-tert-butyl-4-hydroxyphenyl)-propionic acid chloride

: 23128-75-8
3-(3,5-Di-tert-butyl-4-hydroxy-phenyl)-N-{2-[3-(3,5-di-tert-butyl-4-hydroxy-phenyl)-propionylamino]-ethyl}-propionamide

Guidance literature:: With dibutyltin dilaurate; In toluene; at 40 ℃; for 15h; Inert atmosphere;
DOI:10.1134/S1070363216120422

Reference yield:

: 6386-38-5
methyl 3-(4-hydroxy-3,5-di-tert-butyl)phenylpropanoate

: 23128-75-8
3-(3,5-Di-tert-butyl-4-hydroxy-phenyl)-N-{2-[3-(3,5-di-tert-butyl-4-hydroxy-phenyl)-propionylamino]-ethyl}-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 10 h / 60 °C / Inert atmosphere

2: pyrographite / 5,5-dimethyl-1,3-cyclohexadiene / 10 h / 140 °C / Inert atmosphere

With pyrographite; In methanol; 5,5-dimethyl-1,3-cyclohexadiene;