C₁₂H₁₂Cl₃N₃

Base Information

Chemical Name:C₁₂H₁₂Cl₃N₃
CAS No.:1268245-67-5
Molecular Formula:C₁₂H₁₂Cl₃N₃
Molecular Weight:304.606
Hs Code.:

C<sub>12</sub>H<sub>12</sub>Cl<sub>3</sub>N<sub>3</sub>

Synonyms:C₁₂H₁₂Cl₃N₃

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Chemical Property of C₁₂H₁₂Cl₃N₃

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Technology Process of C₁₂H₁₂Cl₃N₃

There total 6 articles about C₁₂H₁₂Cl₃N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.1%

: 1268245-64-2
C₁₂H₁₃Cl₂N₃O

: 1268245-67-5
C₁₂H₁₂Cl₃N₃

Guidance literature:: With tetrachloromethane; triphenylphosphine; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 19393-92-1
1-bromo-2,6-dichlorobenzene

: 1268245-67-5
C₁₂H₁₂Cl₃N₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / triphenylphosphine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 24 h / Reflux; seal tube; Inert atmosphere

2.1: potassium carbonate; methanol / 20 °C / Inert atmosphere

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: 4 h / -78 °C

4.1: 24 h / 110 °C / autoclave

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Cooling with ice

6.1: triphenylphosphine; tetrachloromethane / dichloromethane / 2 h / 20 °C

With methanol; tetrachloromethane; lithium aluminium tetrahydride; n-butyllithium; potassium carbonate; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 6575-25-3
1,3-dichloro-2-ethynyl-benzene

: 1268245-67-5
C₁₂H₁₂Cl₃N₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 4 h / -78 °C

2.1: 24 h / 110 °C / autoclave

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Cooling with ice

4.1: triphenylphosphine; tetrachloromethane / dichloromethane / 2 h / 20 °C

With tetrachloromethane; lithium aluminium tetrahydride; n-butyllithium; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane;