2-chloro-N-<2-(2-chlorobenzoyl)-4-chlorophenyl>-N-(1,1-dimethylethyl)acetamide

Base Information

• Chemical Name: 2-chloro-N-<2-(2-chlorobenzoyl)-4-chlorophenyl>-N-(1,1-dimethylethyl)acetamide
• CAS No.: 126377-87-5
• Molecular Formula: C₁₉H₁₈Cl₃NO₂
• Molecular Weight: 398.716

Synonyms:2-chloro-N-<2-(2-chlorobenzoyl)-4-chlorophenyl>-N-(1,1-dimethylethyl)acetamide

Chemical Property of 2-chloro-N-<2-(2-chlorobenzoyl)-4-chlorophenyl>-N-(1,1-dimethylethyl)acetamide

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Technology Process of 2-chloro-N-<2-(2-chlorobenzoyl)-4-chlorophenyl>-N-(1,1-dimethylethyl)acetamide

There total 2 articles about 2-chloro-N-<2-(2-chlorobenzoyl)-4-chlorophenyl>-N-(1,1-dimethylethyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

<5-chloro-2-<(1,1-dimethylethyl)amino>phenyl>(2-chlorophenyl)methanone (126377-84-2) + chloroacetyl chloride (79-04-9) → 2-chloro-N-<2-(2-chlorobenzoyl)-4-chlorophenyl>-N-(1,1-dimethylethyl)acetamide (126377-87-5)

Guidance literature:

In toluene; for 6h; Heating;

Reference yield:

(2-amino-5-chloro-phenyl)-(2-chloro-phenyl)-methanone (2958-36-3,53960-29-5) → 2-chloro-N-<2-(2-chlorobenzoyl)-4-chlorophenyl>-N-(1,1-dimethylethyl)acetamide (126377-87-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 10 N ethanolic HCl / 11 h / Heating

2: 78 percent / toluene / 6 h / Heating

With hydrogenchloride; In toluene;

Reference yield: 63.0%

2-chloro-N-<2-(2-chlorobenzoyl)-4-chlorophenyl>-N-(1,1-dimethylethyl)acetamide (126377-87-5) → 2-azido-N-<4-chloro-2-(2-chlorobenzoyl)phenyl>-N-(1,1-dimethylethyl)acetamide (126377-89-7)

Guidance literature:

With sodium azide; sodium iodide; In N,N-dimethyl-formamide; for 168h; Ambient temperature;

upstream raw materials:

<5-chloro-2-<(1,1-dimethylethyl)amino>phenyl>(2-chlorophenyl)methanone

chloroacetyl chloride

(2-amino-5-chloro-phenyl)-(2-chloro-phenyl)-methanone

Downstream raw materials:

2-azido-N-<4-chloro-2-(2-chlorobenzoyl)phenyl>-N-(1,1-dimethylethyl)acetamide

7-chloro-5-(2-chlorophenyl)-1,3-dihydro-1-(1,1-dimethylethyl)-2H-1,4-benzodiazepin-2-one

7-chloro-5-(2-chlorophenyl)-1,3,4,5-tetrahydro-1-(1,1-dimethylethyl)-2H-1,4-benzodiazepin-2-one

(R)-7-chloro-5-(2-chlorophenyl)-1,3,4,5-tetrahydro-1-(1,1-dimethylethyl)-2H-1,4-benzodiazepin-2-one

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