(Z)-2-(Benzhydrylidene-amino)-pent-2-enedioic acid 1-tert-butyl ester 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl] ester

Base Information

Chemical Name:(Z)-2-(Benzhydrylidene-amino)-pent-2-enedioic acid 1-tert-butyl ester 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl] ester
CAS No.:342376-59-4
Molecular Formula:C₃₈H₄₅NO₄
Molecular Weight:579.78
Hs Code.:

Synonyms:(Z)-2-(Benzhydrylidene-amino)-pent-2-enedioic acid 1-tert-butyl ester 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl] ester

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Chemical Property of (Z)-2-(Benzhydrylidene-amino)-pent-2-enedioic acid 1-tert-butyl ester 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl] ester

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Technology Process of (Z)-2-(Benzhydrylidene-amino)-pent-2-enedioic acid 1-tert-butyl ester 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl] ester

There total 2 articles about (Z)-2-(Benzhydrylidene-amino)-pent-2-enedioic acid 1-tert-butyl ester 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81477-94-3
N-(diphenylmethylene)glycine tert-butyl ester

: 342376-59-4
(Z)-2-(Benzhydrylidene-amino)-pent-2-enedioic acid 1-tert-butyl ester 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: KOtBu / tetrahydrofuran / 0.5 h / -78 °C

2: LDA / tetrahydrofuran

With potassium tert-butylate; lithium diisopropyl amide; In tetrahydrofuran; 1: Michael addition/1,3-prototropic shift;
DOI:10.1016/S0040-4039(01)00147-2

Reference yield:

: 65253-04-5
(-)-8-phenylmenthol

: 434331-68-7
2-(benzhydrylidene-amino)-pent-2-enedioic acid 1-tert-butyl ester 5-methyl ester

: 342376-59-4
(Z)-2-(Benzhydrylidene-amino)-pent-2-enedioic acid 1-tert-butyl ester 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl] ester

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/S0040-4039(01)00147-2

Reference yield: 50.0%

: 342376-59-4
(Z)-2-(Benzhydrylidene-amino)-pent-2-enedioic acid 1-tert-butyl ester 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl] ester

: 74-88-4
methyl iodide

: (Z)-2-(Benzhydrylidene-amino)-4-methyl-pent-2-enedioic acid 1-tert-butyl ester 5-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl] ester

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1016/S0040-4039(01)00147-2