N,N-dimethyl-1-[5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine

Base Information

Chemical Name:N,N-dimethyl-1-[5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine
CAS No.:1349171-43-2
Molecular Formula:C₁₆H₂₆BNO₂
Molecular Weight:275.199
Hs Code.:

Synonyms:N,N-dimethyl-1-[5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-dimethyl-1-[5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine

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Technology Process of N,N-dimethyl-1-[5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine

There total 2 articles about N,N-dimethyl-1-[5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 23879-32-5
N,N,3-trimethylbenzylamine

: 73183-34-3
bis(pinacol)diborane

: 1349171-43-2
N,N-dimethyl-1-[5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine

Guidance literature:: With methoxy(cyclooctadiene)rhodium(I) dimer; In hexane; at 70 ℃; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja208364a

Reference yield: 55.0%

: 23879-32-5
N,N,3-trimethylbenzylamine

: 73183-34-3
bis(pinacol)diborane

: 1349171-43-2
N,N-dimethyl-1-[5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine

: C₁₆H₂₆BNO₂

: C₂₂H₃₇B₂NO₄

Guidance literature:: With 2-(Aminomethyl)pyridine; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; In methyl cyclohexane; at 70 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol301635x

Reference yield: 72.0%

: 1349171-43-2
N,N-dimethyl-1-[5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanamine

: 62-53-3
aniline

: 2-((dimethylamino)methyl)-4-methyl-N-phenylaniline

Guidance literature:: With potassium fluoride; oxygen; copper(II) acetate monohydrate; In acetonitrile; at 80 ℃; for 2h; Reagent/catalyst; chemoselective reaction; Schlenk technique; Molecular sieve;
DOI:10.1021/acs.joc.5b01074