2-(2,6-dimethoxy-4-(2-methyloctan-2-yl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(2,6-dimethoxy-4-(2-methyloctan-2-yl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1309372-74-4
Molecular Formula:C₂₃H₃₉BO₄
Molecular Weight:390.371
Hs Code.:

Synonyms:2-(2,6-dimethoxy-4-(2-methyloctan-2-yl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-(2,6-dimethoxy-4-(2-methyloctan-2-yl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(2,6-dimethoxy-4-(2-methyloctan-2-yl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 1 articles about 2-(2,6-dimethoxy-4-(2-methyloctan-2-yl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 60526-81-0
1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene

: 1309372-74-4
2-(2,6-dimethoxy-4-(2-methyloctan-2-yl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 1h; Inert atmosphere;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

Reference yield:

: 1309372-76-6
methyl (1R,4S)-7,7-dimethyl-2-(trifluoromethylsulfonyloxy)bicyclo[2.2.1]hept-2-ene-1-carboxylate

: 1309372-74-4
2-(2,6-dimethoxy-4-(2-methyloctan-2-yl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1309372-77-7
HU 911

Guidance literature:: With tetrabutyl ammonium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 15h; Inert atmosphere; Reflux;

Reference yield:

: 1309372-74-4
2-(2,6-dimethoxy-4-(2-methyloctan-2-yl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1309372-83-5
HU 909

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 15 h / Inert atmosphere; Reflux

2: lithium aluminium tetrahydride / diethyl ether; tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; 1: Suzuki Coupling;