6-benzenesulfonyl-6-carbomethoxyhexanoic acid

Base Information

Chemical Name:6-benzenesulfonyl-6-carbomethoxyhexanoic acid
CAS No.:68726-89-6
Molecular Formula:C₁₄H₁₈O₆S
Molecular Weight:314.359
Hs Code.:

Synonyms:6-benzenesulfonyl-6-carbomethoxyhexanoic acid

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Chemical Property of 6-benzenesulfonyl-6-carbomethoxyhexanoic acid

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Technology Process of 6-benzenesulfonyl-6-carbomethoxyhexanoic acid

There total 4 articles about 6-benzenesulfonyl-6-carbomethoxyhexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.5%

: 73842-80-5
2-Benzenesulfonyl-heptanedioic acid 1-methyl ester 7-(2,2,2-trichloro-ethyl) ester

: 68726-89-6
6-benzenesulfonyl-6-carbomethoxyhexanoic acid

Guidance literature:: With acetic acid; zinc; In N,N-dimethyl-formamide; at 0 ℃; for 0.75h;
DOI:10.1021/ja00534a030

Reference yield:

: 2067-33-6
5-bromopentanoic acid

: 68726-89-6
6-benzenesulfonyl-6-carbomethoxyhexanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 1.) room temperature, 45 min, 2.) 45 deg C, 2 h

2: 91 percent / pyridine / CH₂Cl₂ / 1 h / Ambient temperature

3: 82 percent / dimethylsulfoxide / 1 h / Ambient temperature

4: 70.5 percent / zinc, acetic acid / dimethylformamide / 0.75 h / 0 °C

With pyridine; thionyl chloride; acetic acid; zinc; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja00534a030

Reference yield:

: 4509-90-4
5-bromovaleroyl chloride

: 68726-89-6
6-benzenesulfonyl-6-carbomethoxyhexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / pyridine / CH₂Cl₂ / 1 h / Ambient temperature

2: 82 percent / dimethylsulfoxide / 1 h / Ambient temperature

3: 70.5 percent / zinc, acetic acid / dimethylformamide / 0.75 h / 0 °C

With pyridine; acetic acid; zinc; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja00534a030