1,14-tetradecanedicarboxylic acid monochloride monobenzyl ester

Base Information

• Chemical Name: 1,14-tetradecanedicarboxylic acid monochloride monobenzyl ester
• CAS No.: 362707-53-7
• Molecular Formula: C₂₃H₃₅ClO₃
• Molecular Weight: 394.982
• Mol file: 362707-53-7.mol

Synonyms:1,14-tetradecanedicarboxylic acid monochloride monobenzyl ester

Chemical Property of 1,14-tetradecanedicarboxylic acid monochloride monobenzyl ester

Chemical Property:

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Technology Process of 1,14-tetradecanedicarboxylic acid monochloride monobenzyl ester

There total 1 articles about 1,14-tetradecanedicarboxylic acid monochloride monobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

16-(benzyloxy)-16-oxohexadecanoic acid (146004-98-0) → 1,14-tetradecanedicarboxylic acid monochloride monobenzyl ester (362707-53-7)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; for 1h; Heating / reflux;

Reference yield: 61.0%

2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl azide + 1,14-tetradecanedicarboxylic acid monochloride monobenzyl ester (362707-53-7) → N-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)tetradecane-1-carboxamide-14-carboxyl benzyl ester

Guidance literature:

2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl azide; With hydrogen; platinum(IV) oxide; In methanol; at 20 ℃; for 2h;

1,14-tetradecanedicarboxylic acid monochloride monobenzyl ester; In pyridine; DMF (N,N-dimethyl-formamide); dichloromethane; at -20 - 20 ℃; for 26h;

upstream raw materials:

16-(benzyloxy)-16-oxohexadecanoic acid