2--4-(para-chlorophenyl)-3H-1,5-benzodiazepine

Base Information

Chemical Name:2--4-(para-chlorophenyl)-3H-1,5-benzodiazepine
CAS No.:122503-39-3
Molecular Formula:C₂₃H₂₀ClN₃O
Molecular Weight:389.884
Hs Code.:

2-<ortho-methoxy-(N-methylanilino)>-4-(para-chlorophenyl)-3H-1,5-benzodiazepine

Synonyms:2--4-(para-chlorophenyl)-3H-1,5-benzodiazepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--4-(para-chlorophenyl)-3H-1,5-benzodiazepine

Chemical Property:

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Technology Process of 2--4-(para-chlorophenyl)-3H-1,5-benzodiazepine

There total 1 articles about 2--4-(para-chlorophenyl)-3H-1,5-benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 81904-81-6
2-(ortho-methoxyanilino)-4-(p-chlorophenyl)-3H-1,5-benzodiazepine

: 74-88-4
methyl iodide

: 122503-39-3
2--4-(para-chlorophenyl)-3H-1,5-benzodiazepine

Guidance literature:: With sodium hydride; In benzene; Heating;
DOI:10.1002/jhet.5570260121

Reference yield:

: 38870-89-2
Methoxyacetyl chloride

: 122503-39-3
2--4-(para-chlorophenyl)-3H-1,5-benzodiazepine

: 122503-54-2
2a-(chlorophenyl)-2-methoxy-4--1,2,2a,3-tetrahydroazeto<1,2-a><1,5>benzodiazepin-1-one

: 122503-68-8
2a-(p-chlorophenyl)-2-methoxy-5-(2-methoxyacetyl)-4--1,2,2a,5-tetrahydroazeto<1,2-a><1,5>benzodiazepin-1-one

Guidance literature:: With triethylamine; Yield given. Multistep reaction. Yields of byproduct given; 1.) benzene, reflux, 2 h, 2.) benzene, heating, 2 h;
DOI:10.1002/jhet.5570260121