2-(1-((tert-butyl(dimethyl)silyl)oxy)-3-(1-cyclohexenyl)-2-propynyl)quinoxaline

Base Information

Chemical Name:2-(1-((tert-butyl(dimethyl)silyl)oxy)-3-(1-cyclohexenyl)-2-propynyl)quinoxaline
CAS No.:949101-31-9
Molecular Formula:C₂₃H₃₀N₂OSi
Molecular Weight:378.589
Hs Code.:

Synonyms:2-(1-((tert-butyl(dimethyl)silyl)oxy)-3-(1-cyclohexenyl)-2-propynyl)quinoxaline

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Chemical Property of 2-(1-((tert-butyl(dimethyl)silyl)oxy)-3-(1-cyclohexenyl)-2-propynyl)quinoxaline

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Technology Process of 2-(1-((tert-butyl(dimethyl)silyl)oxy)-3-(1-cyclohexenyl)-2-propynyl)quinoxaline

There total 3 articles about 2-(1-((tert-butyl(dimethyl)silyl)oxy)-3-(1-cyclohexenyl)-2-propynyl)quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1044500-74-4
C₁₇H₁₆N₂O

: 18162-48-6
tert-butyldimethylsilyl chloride

: 949101-31-9
2-(1-((tert-butyl(dimethyl)silyl)oxy)-3-(1-cyclohexenyl)-2-propynyl)quinoxaline

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ol701464j

Reference yield:

: 1593-08-4
Quinoxaline-2-carboxaldehyde

: 949101-31-9
2-(1-((tert-butyl(dimethyl)silyl)oxy)-3-(1-cyclohexenyl)-2-propynyl)quinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1.1: MeMgBr / tetrahydrofuran; hexane / 2 h / -78 - 20 °C

1.2: tetrahydrofuran; hexane / 2 h / 20 °C

2.1: imidazole / CH₂Cl₂ / 1 h / 20 °C

With 1H-imidazole; methylmagnesium bromide; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol701464j

Reference yield:

: 931-49-7
1-ethenylcyclohexene

: 949101-31-9
2-(1-((tert-butyl(dimethyl)silyl)oxy)-3-(1-cyclohexenyl)-2-propynyl)quinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1.1: MeMgBr / tetrahydrofuran; hexane / 2 h / -78 - 20 °C

1.2: tetrahydrofuran; hexane / 2 h / 20 °C

2.1: imidazole / CH₂Cl₂ / 1 h / 20 °C

With 1H-imidazole; methylmagnesium bromide; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol701464j