2-(diphenylphosphanyl)-1-{3-[2-(diphenylphosphanyl)-1H-imidazol-1-yl]phenyl}-1H-imidazole

Base Information

Chemical Name:2-(diphenylphosphanyl)-1-{3-[2-(diphenylphosphanyl)-1H-imidazol-1-yl]phenyl}-1H-imidazole
CAS No.:1415966-23-2
Molecular Formula:C₃₆H₂₈N₄P₂
Molecular Weight:578.593
Hs Code.:

Synonyms:2-(diphenylphosphanyl)-1-{3-[2-(diphenylphosphanyl)-1H-imidazol-1-yl]phenyl}-1H-imidazole

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Chemical Property of 2-(diphenylphosphanyl)-1-{3-[2-(diphenylphosphanyl)-1H-imidazol-1-yl]phenyl}-1H-imidazole

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Technology Process of 2-(diphenylphosphanyl)-1-{3-[2-(diphenylphosphanyl)-1H-imidazol-1-yl]phenyl}-1H-imidazole

There total 1 articles about 2-(diphenylphosphanyl)-1-{3-[2-(diphenylphosphanyl)-1H-imidazol-1-yl]phenyl}-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 69506-91-8
1,3-bis(1H-imidazol-1-yl)benzene

: 1415966-23-2
2-(diphenylphosphanyl)-1-{3-[2-(diphenylphosphanyl)-1H-imidazol-1-yl]phenyl}-1H-imidazole

Guidance literature:: 1,3-bis(1H-imidazol-1-yl)benzene; With n-butyllithium; In tetrahydrofuran; hexane; at -20 ℃; for 2h; Inert atmosphere;

chloro-diphenylphosphine; In tetrahydrofuran; hexane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ic3006508

Reference yield: 95.0%

: 1415966-23-2
2-(diphenylphosphanyl)-1-{3-[2-(diphenylphosphanyl)-1H-imidazol-1-yl]phenyl}-1H-imidazole

: 333-27-7
methyl trifluoromethanesulfonate

: 2-(diphenylphosphanyl)-1-{3-[2-(diphenylphosphanyl)-3-methyl-1H-imidazol-3-ium-1 yl]phenyl}-3-methyl-1H-imidazol-3-ium bistriflate

Guidance literature:: In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ic3006508

Reference yield: 89.0%

: 12112-67-3
bis(1,5-cyclooctadiene)diiridium(I) dichloride

: 201230-82-2
carbon monoxide

: 1415966-23-2
2-(diphenylphosphanyl)-1-{3-[2-(diphenylphosphanyl)-1H-imidazol-1-yl]phenyl}-1H-imidazole

: C₃₇H₂₈ClIrN₄OP₂

Guidance literature:: bis(1,5-cyclooctadiene)diiridium(I) dichloride; carbon monoxide; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

2-(diphenylphosphanyl)-1-{3-[2-(diphenylphosphanyl)-1H-imidazol-1-yl]phenyl}-1H-imidazole; In dichloromethane; for 2.5h; Inert atmosphere;
DOI:10.1016/j.molcata.2015.11.005