6-methylamino-9-[(5'-O-benzoyl-2',3'-O-isopropylidene)-4'-thio-β-D-ribofuranosyl]purine

Base Information

Chemical Name:6-methylamino-9-[(5'-O-benzoyl-2',3'-O-isopropylidene)-4'-thio-β-D-ribofuranosyl]purine
CAS No.:1203544-68-6
Molecular Formula:C₂₁H₂₃N₅O₄S
Molecular Weight:441.511
Hs Code.:

Synonyms:6-methylamino-9-[(5'-O-benzoyl-2',3'-O-isopropylidene)-4'-thio-β-D-ribofuranosyl]purine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-methylamino-9-[(5'-O-benzoyl-2',3'-O-isopropylidene)-4'-thio-β-D-ribofuranosyl]purine

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Technology Process of 6-methylamino-9-[(5'-O-benzoyl-2',3'-O-isopropylidene)-4'-thio-β-D-ribofuranosyl]purine

There total 1 articles about 6-methylamino-9-[(5'-O-benzoyl-2',3'-O-isopropylidene)-4'-thio-β-D-ribofuranosyl]purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 900810-19-7
benzoic acid (3aS,4R,6R,6aR)-6-(6-chloro-purin-9-yl)-2,2-dimethyl-tetrahydro-thieno[3,4-d][1,3]dioxol-4-ylmethyl ester

: 593-51-1
methylamine hydrochloride

: 1203544-68-6
6-methylamino-9-[(5'-O-benzoyl-2',3'-O-isopropylidene)-4'-thio-β-D-ribofuranosyl]purine

Guidance literature:: With triethylamine; In ethanol; at 20 ℃; for 24h;
DOI:10.1016/j.bmc.2009.10.011

Reference yield:

: 1203544-68-6
6-methylamino-9-[(5'-O-benzoyl-2',3'-O-isopropylidene)-4'-thio-β-D-ribofuranosyl]purine

: C₁₈H₁₉N₅O₄S

Guidance literature:: 6-methylamino-9-[(5'-O-benzoyl-2',3'-O-isopropylidene)-4'-thio-β-D-ribofuranosyl]purine; With water; acetic acid; at 70 ℃; for 12h;

With ammonia; In methanol;
DOI:10.1016/j.bmc.2009.10.011