N-methyl-N-(4-chlorobutyl) O-(4-carboxyallylmethyl)phenyl phosphoramidic chloride

Base Information

Chemical Name:N-methyl-N-(4-chlorobutyl) O-(4-carboxyallylmethyl)phenyl phosphoramidic chloride
CAS No.:365432-19-5
Molecular Formula:C₁₆H₂₂Cl₂NO₄P
Molecular Weight:394.235
Hs Code.:

Synonyms:N-methyl-N-(4-chlorobutyl) O-(4-carboxyallylmethyl)phenyl phosphoramidic chloride

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Chemical Property of N-methyl-N-(4-chlorobutyl) O-(4-carboxyallylmethyl)phenyl phosphoramidic chloride

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Technology Process of N-methyl-N-(4-chlorobutyl) O-(4-carboxyallylmethyl)phenyl phosphoramidic chloride

There total 3 articles about N-methyl-N-(4-chlorobutyl) O-(4-carboxyallylmethyl)phenyl phosphoramidic chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 208932-52-9
allyl (4-hydroxy)phenylacetate

: 365432-22-0
N-methyl-N-(4-chlorobutyl)phosphoramidic dichloride

: 365432-19-5
N-methyl-N-(4-chlorobutyl) O-(4-carboxyallylmethyl)phenyl phosphoramidic chloride

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -15 - -5 ℃; for 4h;
DOI:10.1021/jm060142p

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 365432-19-5
N-methyl-N-(4-chlorobutyl) O-(4-carboxyallylmethyl)phenyl phosphoramidic chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / diisopropylethylamine / 2 h / Heating

2: 32 percent / diisopropylethylamine / CH₂Cl₂ / 4 h / -15 - -5 °C

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm060142p

Reference yield:

: N-methyl-N-(4-chloro-n-butyl)amine hydrochloride

: 365432-19-5
N-methyl-N-(4-chlorobutyl) O-(4-carboxyallylmethyl)phenyl phosphoramidic chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / POCl₃; Et₃N / CH₂Cl₂ / 20 °C

2: 32 percent / diisopropylethylamine / CH₂Cl₂ / 4 h / -15 - -5 °C

With triethylamine; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In dichloromethane;
DOI:10.1021/jm060142p