3,5-bis{3-[3,5-bis(3-tert-butyloxycarbonylamino-propyl)benzoylamino]propyl}benzoic acid 2,5-dioxopyrrolidin-1-yl ester

Base Information

• Chemical Name: 3,5-bis{3-[3,5-bis(3-tert-butyloxycarbonylamino-propyl)benzoylamino]propyl}benzoic acid 2,5-dioxopyrrolidin-1-yl ester
• CAS No.: 714276-64-9
• Molecular Formula: C₆₃H₉₁N₇O₁₄
• Molecular Weight: 1170.45

Synonyms:3,5-bis{3-[3,5-bis(3-tert-butyloxycarbonylamino-propyl)benzoylamino]propyl}benzoic acid 2,5-dioxopyrrolidin-1-yl ester

Chemical Property of 3,5-bis{3-[3,5-bis(3-tert-butyloxycarbonylamino-propyl)benzoylamino]propyl}benzoic acid 2,5-dioxopyrrolidin-1-yl ester

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Technology Process of 3,5-bis{3-[3,5-bis(3-tert-butyloxycarbonylamino-propyl)benzoylamino]propyl}benzoic acid 2,5-dioxopyrrolidin-1-yl ester

There total 1 articles about 3,5-bis{3-[3,5-bis(3-tert-butyloxycarbonylamino-propyl)benzoylamino]propyl}benzoic acid 2,5-dioxopyrrolidin-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) + 3,5-bis{3-[3,5-bis(3-tert-butyloxycarbonylamino-propyl)benzoylamino]propyl}benzoic acid (349560-06-1) → 3,5-bis{3-[3,5-bis(3-tert-butyloxycarbonylamino-propyl)benzoylamino]propyl}benzoic acid 2,5-dioxopyrrolidin-1-yl ester (714276-64-9)

Guidance literature:

With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1002/chem.200305142

Reference yield: 91.0%

3,5-bis(3-aminopropyl)benzyl alcohol dihydrochloride + 3,5-bis{3-[3,5-bis(3-tert-butyloxycarbonylamino-propyl)benzoylamino]propyl}benzoic acid 2,5-dioxopyrrolidin-1-yl ester (714276-64-9) → 3,5-bis{3-[3,5-bis(3-{3,5-bis(tert-butyloxycarbonylaminopropyl)benzoylamino}propyl)benzoylamino]propyl}benzyl alcohol

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1002/chem.200305142

Reference yield: 87.0%

3,5-bis-(3-amino-propyl)-benzoic acid ethyl ester; compound with trifluoro-acetic acid + 3,5-bis{3-[3,5-bis(3-tert-butyloxycarbonylamino-propyl)benzoylamino]propyl}benzoic acid 2,5-dioxopyrrolidin-1-yl ester (714276-64-9) → ethyl 3,5-bis{3-{{3,5-bis{3-{{3,5-bis{3-{[(tert-butoxy)carbonyl]amino}propyl}benzoyl}amino}propyl}benzoyl}amino}propyl}benzoate (714276-61-6)

Guidance literature:

With TEA; In dichloromethane; at 20 ℃;

DOI:10.1021/ja0494205

upstream raw materials:

1-hydroxy-pyrrolidine-2,5-dione

3,5-bis{3-[3,5-bis(3-tert-butyloxycarbonylamino-propyl)benzoylamino]propyl}benzoic acid

Downstream raw materials:

ethyl 3,5-bis{3-{{3,5-bis{3-{{3,5-bis{3-{[(tert-butoxy)carbonyl]amino}propyl}benzoyl}amino}propyl}benzoyl}amino}propyl}benzoate

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