N,N'-(6-(4-((trimethylsilyl)ethynyl)phenyl)-1,3,5-triazine-2,4-diyl)dipropionamide

Base Information

Chemical Name:N,N'-(6-(4-((trimethylsilyl)ethynyl)phenyl)-1,3,5-triazine-2,4-diyl)dipropionamide
CAS No.:1268611-42-2
Molecular Formula:C₂₀H₂₅N₅O₂Si
Molecular Weight:395.536
Hs Code.:

Synonyms:N,N'-(6-(4-((trimethylsilyl)ethynyl)phenyl)-1,3,5-triazine-2,4-diyl)dipropionamide

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Chemical Property of N,N'-(6-(4-((trimethylsilyl)ethynyl)phenyl)-1,3,5-triazine-2,4-diyl)dipropionamide

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Technology Process of N,N'-(6-(4-((trimethylsilyl)ethynyl)phenyl)-1,3,5-triazine-2,4-diyl)dipropionamide

There total 3 articles about N,N'-(6-(4-((trimethylsilyl)ethynyl)phenyl)-1,3,5-triazine-2,4-diyl)dipropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1268611-38-6
N,N'-(6-(4-bromophenyl)-1,3,5-triazine-2,4-diyl)dipropionamide

: 1066-54-2
trimethylsilylacetylene

: 1268611-42-2
N,N'-(6-(4-((trimethylsilyl)ethynyl)phenyl)-1,3,5-triazine-2,4-diyl)dipropionamide

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In tetrahydrofuran; at 50 ℃; for 72h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2010.09.047

Reference yield:

: 623-00-7
4-bromobenzenecarbonitrile

: 1268611-42-2
N,N'-(6-(4-((trimethylsilyl)ethynyl)phenyl)-1,3,5-triazine-2,4-diyl)dipropionamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / 2-ethoxy-ethanol / 24 h / Reflux

2: pyridine / 72 h / Reflux

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / tetrahydrofuran / 72 h / 50 °C / Inert atmosphere

With pyridine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; potassium hydroxide; In tetrahydrofuran; 2-ethoxy-ethanol; 3: Sonogashira coupling;
DOI:10.1016/j.jorganchem.2010.09.047

Reference yield:

: 30508-74-8
6-(4-bromophenyl)-1,3,5-triazine-2,4-diamine

: 1268611-42-2
N,N'-(6-(4-((trimethylsilyl)ethynyl)phenyl)-1,3,5-triazine-2,4-diyl)dipropionamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 72 h / Reflux

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / tetrahydrofuran / 72 h / 50 °C / Inert atmosphere

With pyridine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In tetrahydrofuran; 2: Sonogashira coupling;
DOI:10.1016/j.jorganchem.2010.09.047