1-α-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-L-alanyl-D-glutamine n-propyl ester

Base Information

Chemical Name:1-α-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-L-alanyl-D-glutamine n-propyl ester
CAS No.:79787-39-6
Molecular Formula:C₃₆H₄₈N₄O₁₁
Molecular Weight:712.797
Hs Code.:

Synonyms:1-α-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-L-alanyl-D-glutamine n-propyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-α-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-L-alanyl-D-glutamine n-propyl ester

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Technology Process of 1-α-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-L-alanyl-D-glutamine n-propyl ester

There total 3 articles about 1-α-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-L-alanyl-D-glutamine n-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5959-95-5,26700-71-0
D-Glutamin

: 79787-39-6
1-α-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-L-alanyl-D-glutamine n-propyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Et₃N, 2.) dimethylaminopropylamine / 1.) THF, H₂O, 4 deg C, 24 h, 2.) THF, H₂O, 1 h

2: 1.) aq. Cs₂CO₃ / 1.) THF, 2.) DMF, RT, 48 h

3: H₂, HOAc, 1 N HCl / 5percent Pd/C / 2 h / 760 Torr

4: N-methylmorpholine, isobutyl chloroformate / dimethylformamide / -15 °C

With 4-methyl-morpholine; hydrogenchloride; hydrogen; caesium carbonate; acetic acid; triethylamine; 1-amino-3-(dimethylamino)propane; isobutyl chloroformate; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1021/jm00343a018

Reference yield:

: 74842-54-9
Cbz-L-Ala-D-Gln

: 79787-39-6
1-α-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-L-alanyl-D-glutamine n-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) aq. Cs₂CO₃ / 1.) THF, 2.) DMF, RT, 48 h

2: H₂, HOAc, 1 N HCl / 5percent Pd/C / 2 h / 760 Torr

3: N-methylmorpholine, isobutyl chloroformate / dimethylformamide / -15 °C

With 4-methyl-morpholine; hydrogenchloride; hydrogen; caesium carbonate; acetic acid; isobutyl chloroformate; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1021/jm00343a018

Reference yield:

: 79787-34-1
Cbz-L-Ala-D-Gln-O-n-C₃H₇

: 79787-39-6
1-α-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-L-alanyl-D-glutamine n-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, HOAc, 1 N HCl / 5percent Pd/C / 2 h / 760 Torr

2: N-methylmorpholine, isobutyl chloroformate / dimethylformamide / -15 °C

With 4-methyl-morpholine; hydrogenchloride; hydrogen; acetic acid; isobutyl chloroformate; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1021/jm00343a018