N-(2-chloro-3-methoxyphenyl)-2-hydroxyiminoacetamide

Base Information

Chemical Name:N-(2-chloro-3-methoxyphenyl)-2-hydroxyiminoacetamide
CAS No.:1180495-72-0
Molecular Formula:C₉H₉ClN₂O₃
Molecular Weight:228.635
Hs Code.:

Synonyms:N-(2-chloro-3-methoxyphenyl)-2-hydroxyiminoacetamide

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Chemical Property of N-(2-chloro-3-methoxyphenyl)-2-hydroxyiminoacetamide

Chemical Property:

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Technology Process of N-(2-chloro-3-methoxyphenyl)-2-hydroxyiminoacetamide

There total 1 articles about N-(2-chloro-3-methoxyphenyl)-2-hydroxyiminoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 302-17-0
chloral hydrate

: 85893-87-4
2-chloro-3-methoxyaniline hydrochloride

: 1180495-72-0
N-(2-chloro-3-methoxyphenyl)-2-hydroxyiminoacetamide

Guidance literature:: With hydrogenchloride; hydroxylamine; sodium sulfate; In water; for 1.5h; Reflux;

Reference yield:

: 1180495-72-0
N-(2-chloro-3-methoxyphenyl)-2-hydroxyiminoacetamide

: 1180495-76-4
methyl 3-chloro-2-(4-isopropylthiazole-2-carboxamido)-4-methoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron trifluoride diethyl etherate / 3 h / 40 - 90 °C

2.1: sodium hydroxide; sodium chloride / water / 0.5 h / 20 °C / Cooling with ice

2.2: 3 h / 0 - 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.2: 2 h / 20 °C

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2.5 h / 0 - 20 °C

4.2: 16 h / 20 °C

With oxalyl dichloride; boron trifluoride diethyl etherate; potassium carbonate; sodium chloride; sodium hydroxide; N,N-dimethyl-formamide; In dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1180495-72-0
N-(2-chloro-3-methoxyphenyl)-2-hydroxyiminoacetamide

: 1180495-74-2
2-amino-3-chloro-4-methoxy benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / 3 h / 40 - 90 °C

2.1: sodium hydroxide; sodium chloride / water / 0.5 h / 20 °C / Cooling with ice

2.2: 3 h / 0 - 20 °C

With boron trifluoride diethyl etherate; sodium chloride; sodium hydroxide; In water;