2-amino-3-chloro-4-methoxy benzoic acid methyl ester

Base Information

Chemical Name:2-amino-3-chloro-4-methoxy benzoic acid methyl ester
CAS No.:1180495-75-3
Molecular Formula:C₉H₁₀ClNO₃
Molecular Weight:215.636
Hs Code.:

Synonyms:2-amino-3-chloro-4-methoxy benzoic acid methyl ester

Suppliers and Price of 2-amino-3-chloro-4-methoxy benzoic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 2-amino-3-chloro-4-methoxy benzoic acid methyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-amino-3-chloro-4-methoxy benzoic acid methyl ester

There total 6 articles about 2-amino-3-chloro-4-methoxy benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1180495-74-2
2-amino-3-chloro-4-methoxy benzoic acid

: 74-88-4
methyl iodide

: 1180495-75-3
2-amino-3-chloro-4-methoxy benzoic acid methyl ester

Guidance literature:: 2-amino-3-chloro-4-methoxy benzoic acid; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

With citric acid; In water; N,N-dimethyl-formamide;

Reference yield: 50.0%

: 1180495-74-2
2-amino-3-chloro-4-methoxy benzoic acid

: 77-92-9,906507-37-7
citric acid

: 74-88-4
methyl iodide

: 1180495-75-3
2-amino-3-chloro-4-methoxy benzoic acid methyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide;

Reference yield:

: 85893-87-4
2-chloro-3-methoxyaniline hydrochloride

: 1180495-75-3
2-amino-3-chloro-4-methoxy benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; hydroxylamine; sodium sulfate / water / 1.5 h / Reflux

2.1: boron trifluoride diethyl etherate / 3 h / 40 - 90 °C

3.1: sodium hydroxide; sodium chloride / water / 0.5 h / 20 °C / Cooling with ice

3.2: 3 h / 0 - 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.2: 2 h / 20 °C

With hydrogenchloride; boron trifluoride diethyl etherate; hydroxylamine; potassium carbonate; sodium sulfate; sodium chloride; sodium hydroxide; In water; N,N-dimethyl-formamide;