N'-(4-chlorophenyl)-2-((8S,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-2-oxoacetohydrazonoyl cyanide

Base Information

Chemical Name:N'-(4-chlorophenyl)-2-((8S,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-2-oxoacetohydrazonoyl cyanide
CAS No.:1534364-08-3
Molecular Formula:C₂₈H₃₂ClN₃O₂
Molecular Weight:478.034
Hs Code.:

N'-(4-chlorophenyl)-2-((8S,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-2-oxoacetohydrazonoyl cyanide

Synonyms:N'-(4-chlorophenyl)-2-((8S,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-2-oxoacetohydrazonoyl cyanide

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Chemical Property of N'-(4-chlorophenyl)-2-((8S,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-2-oxoacetohydrazonoyl cyanide

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Technology Process of N'-(4-chlorophenyl)-2-((8S,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-2-oxoacetohydrazonoyl cyanide

There total 4 articles about N'-(4-chlorophenyl)-2-((8S,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-2-oxoacetohydrazonoyl cyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1534363-79-5
3-((8S,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14, 15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-3-oxopropanenitrile

: 2028-74-2
p-chlorobenzenediazonium chloride

: 1534364-08-3
N'-(4-chlorophenyl)-2-((8S,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-2-oxoacetohydrazonoyl cyanide

Guidance literature:: With sodium acetate; In ethanol; at 20 ℃; for 1h;
DOI:10.1007/s00044-013-0894-8

Reference yield:

: 106-47-8
4-chloro-aniline

: 1534364-08-3
N'-(4-chlorophenyl)-2-((8S,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-2-oxoacetohydrazonoyl cyanide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium nitrite; hydrogenchloride / Cooling

2: sodium acetate / ethanol / 1 h / 20 °C

With hydrogenchloride; sodium acetate; sodium nitrite; In ethanol;
DOI:10.1007/s00044-013-0894-8

Reference yield:

: 57-83-0
Progesterone

: 1534364-08-3
N'-(4-chlorophenyl)-2-((8S,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-2-oxoacetohydrazonoyl cyanide

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; bromine / 1 h / 20 - 60 °C

2: ethanol; water / 2 h / 60 °C

3: sodium acetate / ethanol / 1 h / 20 °C

With bromine; sodium acetate; acetic acid; In ethanol; water;
DOI:10.1007/s00044-013-0894-8