N-(S)-α-methylbenzyl-O-benzoyl hydroxylamine hydrochloride

Base Information

• Chemical Name: N-(S)-α-methylbenzyl-O-benzoyl hydroxylamine hydrochloride
• CAS No.: 1374683-07-4
• Molecular Formula: C₁₅H₁₅NO₂*ClH
• Molecular Weight: 277.751
• Mol file: 1374683-07-4.mol

Synonyms:N-(S)-α-methylbenzyl-O-benzoyl hydroxylamine hydrochloride

Chemical Property of N-(S)-α-methylbenzyl-O-benzoyl hydroxylamine hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(S)-α-methylbenzyl-O-benzoyl hydroxylamine hydrochloride

There total 1 articles about N-(S)-α-methylbenzyl-O-benzoyl hydroxylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) + dibenzoyl peroxide (94-36-0) → N-(S)-α-methylbenzyl-O-benzoyl hydroxylamine hydrochloride (1374683-07-4)

Guidance literature:

(S)-1-phenyl-ethylamine; dibenzoyl peroxide; In dichloromethane; water; at 20 ℃; for 18h; pH=10.5; aq. buffer; Inert atmosphere;

With hydrogenchloride; In diethyl ether; Inert atmosphere;

DOI:10.1039/c2ob25293g

Reference yield: 92.0%

N-(S)-α-methylbenzyl-O-benzoyl hydroxylamine hydrochloride (1374683-07-4) → N-(S)-α-methylbenzyl-O-benzoyl hydroxylamine (1485-74-1,116782-38-8,143678-69-7,105450-03-1)

Guidance literature:

N-(S)-α-methylbenzyl-O-benzoyl hydroxylamine hydrochloride; In dichloromethane; at 20 ℃; for 1h; pH=10.5; Inert atmosphere;

Inert atmosphere;

DOI:10.1039/c2ob25293g

Reference yield: 68.0%

N-(S)-α-methylbenzyl-O-benzoyl hydroxylamine hydrochloride (1374683-07-4) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → 2-benzoyloxycyclohexanone (7472-23-3)

Guidance literature:

In dimethyl sulfoxide; at 25 ℃; Inert atmosphere;

DOI:10.1039/c2ob25293g

upstream raw materials:

(S)-1-phenyl-ethylamine

dibenzoyl peroxide

Downstream raw materials:

N-(S)-α-methylbenzyl-O-benzylcarbonate hydroxylamine

N-(S)-α-methylbenzyl-O-pivaloyl hydroxylamine

N-(S)-α-methylbenzyl-O-diphenylcarbamoyl hydroxylamine

N-(S)-α-methylbenzyl-O-3,5-di-tert-butylbenzoyl hydroxylamine