1-Cyclohexyl-2-methylideneaziridine

Base Information

Chemical Name:1-Cyclohexyl-2-methylideneaziridine
CAS No.:195153-97-0
Molecular Formula:C9H15 N
Molecular Weight:137.225
Hs Code.:
DSSTox Substance ID:DTXSID90440956
Nikkaji Number:J896.607I
Mol file:195153-97-0.mol

Synonyms:1-Cyclohexyl-2-methylideneaziridine;195153-97-0;Aziridine, 1-cyclohexyl-2-methylene- (9CI);DTXSID90440956;1-Cyclohexyl-2-methyleneaziridine

Suppliers and Price of 1-Cyclohexyl-2-methylideneaziridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-Cyclohexyl-2-methylideneaziridine

Chemical Property:

PSA：3.01000
LogP:2.08630
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:137.120449483
Heavy Atom Count:10
Complexity:145

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=C1CN1C2CCCCC2

Technology Process of 1-Cyclohexyl-2-methylideneaziridine

There total 3 articles about 1-Cyclohexyl-2-methylideneaziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 111831-89-1
N-(2-Bromoprop-2-enyl)cyclohexylamine

: 195153-97-0
1-(1-cyclohexyl)-2-methyleneaziridine

Guidance literature:: With sodium amide; In ammonia; for 3h;
DOI:10.1039/b002223n

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 195153-97-0
1-(1-cyclohexyl)-2-methyleneaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / K₂CO₃ / tetrahydrofuran / 31 h / Heating

2: 78 percent / NaNH₂ / liquid ammonia / 3 h

With potassium carbonate; sodium amide; In tetrahydrofuran; ammonia; 1: Alkylation / 2: Cyclization;
DOI:10.1039/b002223n

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 195153-97-0
1-(1-cyclohexyl)-2-methyleneaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

2: ammonia; sodium amide / diethyl ether / 1 h / -78 °C

With ammonia; potassium carbonate; sodium amide; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1039/c3cc41061g