Technology Process of C17H25BO5
There total 5 articles about C17H25BO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; bis(pinacol)diborane;
In
1,4-dioxane;
at 80 ℃;
for 3h;
Inert atmosphere;
- Guidance literature:
-
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate;
In
1,4-dioxane;
at 80 - 85 ℃;
for 8h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / acetonitrile / Reflux
2.1: sulfuric acid / water; acetone / 0 °C
2.2: 5 h / 0 °C
3.1: sulfuric acid / 0 °C / Reflux
4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; bis(pinacol)diborane / 1,4-dioxane / 3 h / 80 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; potassium acetate; potassium carbonate; bis(pinacol)diborane;
In
1,4-dioxane; water; acetone; acetonitrile;