methyl 3-amino-4,6-O-benzylidene-2,3-dideoxy-3-C-methyl-α-D-ribo-hexopyranoside

Base Information

Chemical Name:methyl 3-amino-4,6-O-benzylidene-2,3-dideoxy-3-C-methyl-α-D-ribo-hexopyranoside
CAS No.:98758-29-3
Molecular Formula:C₁₅H₂₁NO₄
Molecular Weight:279.336
Hs Code.:

Synonyms:methyl 3-amino-4,6-O-benzylidene-2,3-dideoxy-3-C-methyl-α-D-ribo-hexopyranoside

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Chemical Property of methyl 3-amino-4,6-O-benzylidene-2,3-dideoxy-3-C-methyl-α-D-ribo-hexopyranoside

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Technology Process of methyl 3-amino-4,6-O-benzylidene-2,3-dideoxy-3-C-methyl-α-D-ribo-hexopyranoside

There total 10 articles about methyl 3-amino-4,6-O-benzylidene-2,3-dideoxy-3-C-methyl-α-D-ribo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 149353-42-4
methyl 4,6-O-benzylidene-2,3-dideoxy-3-(O-benzylhydroxyamino)-3-C-methyl-α-D-ribo-hexopyranoside

: 98758-29-3
methyl 3-amino-4,6-O-benzylidene-2,3-dideoxy-3-C-methyl-α-D-ribo-hexopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 20h; Ambient temperature;
DOI:10.1021/jo00066a029

Reference yield:

: 63598-31-2
methyl 4,6-O-(R)-benzylidene-2-deoxy-α-D-erythrohexopyranosid-3-ulose

: 98758-29-3
methyl 3-amino-4,6-O-benzylidene-2,3-dideoxy-3-C-methyl-α-D-ribo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / ethanol / 2 h / Ambient temperature

2: 1) CeCl₃ / 1) THF, -78 deg C, 1 h, 2) THF, a) -78 deg C, 2 h, b) 0 deg C, 1 h

3: H₂ / 10percent Pd-C / methanol / 20 h / Ambient temperature

With cerium(III) chloride; hydrogen; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jo00066a029

Reference yield:

: O-benzyl methyl 4,6-O-benzylidene-2,3-dideoxy-α-D-erythro-hexopyranosid-3-ulose oxime

: 98758-29-3
methyl 3-amino-4,6-O-benzylidene-2,3-dideoxy-3-C-methyl-α-D-ribo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1) CeCl₃ / 1) THF, -78 deg C, 1 h, 2) THF, a) -78 deg C, 2 h, b) 0 deg C, 1 h

2: H₂ / 10percent Pd-C / methanol / 20 h / Ambient temperature

With cerium(III) chloride; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00066a029