potassium salt of N-diisopropoxythiophosphorylthiobenzamide

Base Information

• Chemical Name: potassium salt of N-diisopropoxythiophosphorylthiobenzamide
• CAS No.: 128342-57-4
• Molecular Formula: C₁₃H₁₉NO₂PS₂*K
• Molecular Weight: 355.503
• Mol file: 128342-57-4.mol

Synonyms:potassium salt of N-diisopropoxythiophosphorylthiobenzamide

Chemical Property of potassium salt of N-diisopropoxythiophosphorylthiobenzamide

Chemical Property:

Purity/Quality:

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Technology Process of potassium salt of N-diisopropoxythiophosphorylthiobenzamide

There total 2 articles about potassium salt of N-diisopropoxythiophosphorylthiobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

N-(diisopropoxythiophosphoryl)thiobenzamide (66078-55-5) → potassium salt of N-diisopropoxythiophosphorylthiobenzamide (128342-57-4)

Guidance literature:

With potassium hydroxide; In methanol; for 2h; Ambient temperature;

Reference yield:

O,O-diisopropyl chlorothiophosphate (2524-06-3) + benzenecarbothioamide (2227-79-4) → potassium salt of N-diisopropoxythiophosphorylthiobenzamide (128342-57-4)

Guidance literature:

With potassium hydroxide; Multistep reaction; 1.) acetone, 2.) 80-100 deg C, 2 h;

Reference yield: 88.5%

1-iodo-butane (542-69-8) + potassium salt of N-diisopropoxythiophosphorylthiobenzamide (128342-57-4) → [1-Butylsulfanyl-1-phenyl-meth-(Z)-ylidene]-thiophosphoramidic acid O,O'-diisopropyl ester

Guidance literature:

In acetone; for 3h; Heating;

upstream raw materials:

N-(diisopropoxythiophosphoryl)thiobenzamide

O,O-diisopropyl chlorothiophosphate

benzenecarbothioamide

Downstream raw materials:

S-tert-butyl N-diisopropoxythiophosphorylbenzimidothioate

N-diisopropoxythiophosphoryl-S-methylbenzimidothioate

potassium N-diisopropoxythiophosphorylbenzamidate