1,2;5,6-di-O-isopropylidene-3-deoxy-3-{[(2-trifluoromethylphenyl)-methyl]carbonyl}-amino-α-D-allofuranoside

Base Information

Chemical Name:1,2;5,6-di-O-isopropylidene-3-deoxy-3-{[(2-trifluoromethylphenyl)-methyl]carbonyl}-amino-α-D-allofuranoside
CAS No.:951775-31-8
Molecular Formula:C₂₁H₂₆F₃NO₆
Molecular Weight:445.436
Hs Code.:

Synonyms:1,2;5,6-di-O-isopropylidene-3-deoxy-3-{[(2-trifluoromethylphenyl)-methyl]carbonyl}-amino-α-D-allofuranoside

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Chemical Property of 1,2;5,6-di-O-isopropylidene-3-deoxy-3-{[(2-trifluoromethylphenyl)-methyl]carbonyl}-amino-α-D-allofuranoside

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Technology Process of 1,2;5,6-di-O-isopropylidene-3-deoxy-3-{[(2-trifluoromethylphenyl)-methyl]carbonyl}-amino-α-D-allofuranoside

There total 4 articles about 1,2;5,6-di-O-isopropylidene-3-deoxy-3-{[(2-trifluoromethylphenyl)-methyl]carbonyl}-amino-α-D-allofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3038-48-0
2-(trifluoromethyl)phenylacetic acid

: 16848-19-4
1,2,5,6-di-O-isopropylidene-3-deoxy-3-amino-α-D-glucofuranoside

: 951775-31-8
1,2;5,6-di-O-isopropylidene-3-deoxy-3-{[(2-trifluoromethylphenyl)-methyl]carbonyl}-amino-α-D-allofuranoside

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 11h;

Reference yield:

: 10578-95-7
(E/Z)-3-Deoxy-3-hydroxyimino-1,2:5,6-di-O-isopropylidene-α-D-ribohexofuranose

: 951775-31-8
1,2;5,6-di-O-isopropylidene-3-deoxy-3-{[(2-trifluoromethylphenyl)-methyl]carbonyl}-amino-α-D-allofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 0 - 20 °C

2.1: 4-methyl-morpholine; benzotriazol-1-ol / N,N-dimethyl-formamide / 1 h / 0 °C

2.2: 10 h / 0 - 20 °C

With 4-methyl-morpholine; lithium aluminium tetrahydride; benzotriazol-1-ol; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 582-52-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 951775-31-8
1,2;5,6-di-O-isopropylidene-3-deoxy-3-{[(2-trifluoromethylphenyl)-methyl]carbonyl}-amino-α-D-allofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic anhydride / dimethyl sulfoxide / 24 h / 50 - 60 °C

2.1: pyridine; hydroxylamine hydrochloride / ethanol / 24.5 h / 20 - 75 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 0 - 20 °C

4.1: 4-methyl-morpholine; benzotriazol-1-ol / N,N-dimethyl-formamide / 1 h / 0 °C

4.2: 10 h / 0 - 20 °C

With 4-methyl-morpholine; pyridine; lithium aluminium tetrahydride; hydroxylamine hydrochloride; acetic anhydride; benzotriazol-1-ol; In tetrahydrofuran; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;