2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-dihydroxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Base Information

Chemical Name:2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-dihydroxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione
CAS No.:110426-19-2
Molecular Formula:C₄₃H₄₉NO₁₂
Molecular Weight:771.862
Hs Code.:

2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-dihydroxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Synonyms:2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-dihydroxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

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Chemical Property of 2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-dihydroxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

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Technology Process of 2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-dihydroxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

There total 5 articles about 2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-dihydroxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 110426-18-1
Acetic acid (2S,3R,4S,5S,6R)-5-acetoxy-4-allyloxy-2-[(2R,3S,4R,5R,6R)-6-allyloxy-4-benzyloxy-2-benzyloxymethyl-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-3-yloxy]-6-allyloxymethyl-tetrahydro-pyran-3-yl ester

: 110426-19-2
2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-dihydroxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Guidance literature:: With lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water;

Reference yield:

: (2R,3S,4S,5R,6R)-4-Allyloxy-2-allyloxymethyl-6-(2,2,2-trichloro-ethoxy)-tetrahydro-pyran-3,5-diol

: 110426-19-2
2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-dihydroxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / various solvent(s)

2: 1.) Zn, AcOH; 2.) SOCl₂ / 2.) DMF / 1.) THF; 2.) CH₂Cl₂

3: 88 percent / AgOTf, MS₄A / 1,2-dichloro-ethane

4: 88 percent / LiOH, 31percent H₂O₂ / tetrahydrofuran; H₂O

With pyridine; lithium hydroxide; thionyl chloride; dihydrogen peroxide; silver trifluoromethanesulfonate; acetic acid; zinc; N,N-dimethyl-formamide; In tetrahydrofuran; water; 1,2-dichloro-ethane;

Reference yield:

: 391859-79-3
Acetic acid (2R,3R,4S,5S,6R)-5-acetoxy-4-allyloxy-6-allyloxymethyl-2-(2,2,2-trichloro-ethoxy)-tetrahydro-pyran-3-yl ester

: 110426-19-2
2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-dihydroxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Zn, AcOH; 2.) SOCl₂ / 2.) DMF / 1.) THF; 2.) CH₂Cl₂

2: 88 percent / AgOTf, MS₄A / 1,2-dichloro-ethane

3: 88 percent / LiOH, 31percent H₂O₂ / tetrahydrofuran; H₂O

With lithium hydroxide; thionyl chloride; dihydrogen peroxide; silver trifluoromethanesulfonate; acetic acid; zinc; N,N-dimethyl-formamide; In tetrahydrofuran; water; 1,2-dichloro-ethane;