2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Base Information

Chemical Name:2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione
CAS No.:110426-16-9
Molecular Formula:C₅₇H₆₁NO₁₂
Molecular Weight:952.111
Hs Code.:

2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Synonyms:2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Suppliers and Price of 2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

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Chemical Property of 2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

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Technology Process of 2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

There total 11 articles about 2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 100-39-0
benzyl bromide

: 110426-19-2
2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-dihydroxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

: 110426-16-9
2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Guidance literature:: With silver(l) oxide; potassium iodide; In N,N-dimethyl-formamide;

Reference yield:

: (2R,3S,4S,5R,6R)-4-Allyloxy-2-allyloxymethyl-6-(2,2,2-trichloro-ethoxy)-tetrahydro-pyran-3,5-diol

: 110426-16-9
2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / various solvent(s)

2: 1.) Zn, AcOH; 2.) SOCl₂ / 2.) DMF / 1.) THF; 2.) CH₂Cl₂

3: 88 percent / AgOTf, MS₄A / 1,2-dichloro-ethane

4: 88 percent / LiOH, 31percent H₂O₂ / tetrahydrofuran; H₂O

5: 94 percent / Ag₂O / KI / dimethylformamide

With pyridine; lithium hydroxide; thionyl chloride; dihydrogen peroxide; silver trifluoromethanesulfonate; acetic acid; silver(l) oxide; zinc; potassium iodide; In tetrahydrofuran; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 110426-17-0
Acetic acid (2R,3S,4S,5R,6R)-5-acetoxy-4-allyloxy-2-allyloxymethyl-6-chloro-tetrahydro-pyran-3-yl ester

: 110426-16-9
2-[(2R,3R,4R,5S,6R)-2-Allyloxy-5-((2S,3R,4S,5S,6R)-4-allyloxy-6-allyloxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / AgOTf, MS₄A / 1,2-dichloro-ethane

2: 88 percent / LiOH, 31percent H₂O₂ / tetrahydrofuran; H₂O

3: 94 percent / Ag₂O / KI / dimethylformamide

With lithium hydroxide; dihydrogen peroxide; silver trifluoromethanesulfonate; silver(l) oxide; potassium iodide; In tetrahydrofuran; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;