C₂₄H₃₈O₆

Base Information

Chemical Name:C₂₄H₃₈O₆
CAS No.:1355239-73-4
Molecular Formula:C₂₄H₃₈O₆
Molecular Weight:422.562
Hs Code.:

C<sub>24</sub>H<sub>38</sub>O<sub>6</sub>

Synonyms:C₂₄H₃₈O₆

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Chemical Property of C₂₄H₃₈O₆

Chemical Property:

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Technology Process of C₂₄H₃₈O₆

There total 13 articles about C₂₄H₃₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 67-56-1
methanol

: 1355239-70-1
C₃₅H₆₄O₆Si₂

: 1355239-73-4
C₂₄H₃₈O₆

Guidance literature:: With 10-camphorsufonic acid; In dichloromethane; at 20 - 25 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ol203342e

Reference yield:

: 1355240-03-7
C₁₄H₁₈O₂

: 1355239-73-4
C₂₄H₃₈O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: zirconocene dichloride; diisobutylaluminium hydride / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere

1.2: 0.17 h / -78 - 0 °C / Inert atmosphere

2.1: tert.-butyl lithium / diethyl ether; pentane / 1.5 h / -78 °C / Inert atmosphere

2.2: -78 - 25 °C / Inert atmosphere

2.3: 4 h / 20 - 25 °C / Inert atmosphere

3.1: water; acetic acid / tetrahydrofuran / 5 h / 50 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere

4.2: 1 h / -78 - 0 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran; hexane / 2.33 h / -78 °C / Inert atmosphere

5.2: 4 h / -78 - 0 °C / Inert atmosphere

5.3: Inert atmosphere

6.1: 1H-imidazole / dichloromethane / 2 h / 0 - 25 °C / Inert atmosphere

7.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

7.2: 2 h / -78 °C / Inert atmosphere

8.1: potassium osmate(VI) dihydrate; methanesulfonamide; water; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III) / tert-butyl alcohol / 60 h / 0 °C / Inert atmosphere

9.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 48 h / 35 °C / Inert atmosphere

10.1: 10-camphorsufonic acid / dichloromethane / 1.5 h / 20 - 25 °C / Inert atmosphere

With 1H-imidazole; potassium osmate(VI) dihydrate; n-butyllithium; zirconocene dichloride; methanesulfonamide; 10-camphorsufonic acid; water; tert.-butyl lithium; sulfur trioxide pyridine complex; sodium hydride; diisobutylaluminium hydride; potassium carbonate; acetic acid; dimethyl sulfoxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; potassium hexacyanoferrate(III); In tetrahydrofuran; diethyl ether; hexane; dichloromethane; mineral oil; tert-butyl alcohol; pentane; 8.1: Sharpless dihydroxylation / 9.1: Parikh-Doering oxidation;
DOI:10.1021/ol203342e

Reference yield:

: 1355240-06-0
C₁₄H₁₉IO₂

: 1355239-73-4
C₂₄H₃₈O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: tert.-butyl lithium / diethyl ether; pentane / 1.5 h / -78 °C / Inert atmosphere

1.2: -78 - 25 °C / Inert atmosphere

1.3: 4 h / 20 - 25 °C / Inert atmosphere

2.1: water; acetic acid / tetrahydrofuran / 5 h / 50 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere

3.2: 1 h / -78 - 0 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 2.33 h / -78 °C / Inert atmosphere

4.2: 4 h / -78 - 0 °C / Inert atmosphere

4.3: Inert atmosphere

5.1: 1H-imidazole / dichloromethane / 2 h / 0 - 25 °C / Inert atmosphere

6.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

6.2: 2 h / -78 °C / Inert atmosphere

7.1: potassium osmate(VI) dihydrate; methanesulfonamide; water; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III) / tert-butyl alcohol / 60 h / 0 °C / Inert atmosphere

8.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 48 h / 35 °C / Inert atmosphere

9.1: 10-camphorsufonic acid / dichloromethane / 1.5 h / 20 - 25 °C / Inert atmosphere

With 1H-imidazole; potassium osmate(VI) dihydrate; n-butyllithium; methanesulfonamide; 10-camphorsufonic acid; water; tert.-butyl lithium; sulfur trioxide pyridine complex; sodium hydride; potassium carbonate; acetic acid; dimethyl sulfoxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; potassium hexacyanoferrate(III); In tetrahydrofuran; diethyl ether; hexane; dichloromethane; mineral oil; tert-butyl alcohol; pentane; 7.1: Sharpless dihydroxylation / 8.1: Parikh-Doering oxidation;
DOI:10.1021/ol203342e