2-(4-methoxy-2-(methoxymethoxy)phenyl)-2-(trimethylsilyloxy)acetonitrile

Base Information

Chemical Name:2-(4-methoxy-2-(methoxymethoxy)phenyl)-2-(trimethylsilyloxy)acetonitrile
CAS No.:1163251-97-5
Molecular Formula:C₁₄H₂₁NO₄Si
Molecular Weight:295.411
Hs Code.:

Synonyms:2-(4-methoxy-2-(methoxymethoxy)phenyl)-2-(trimethylsilyloxy)acetonitrile

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Chemical Property of 2-(4-methoxy-2-(methoxymethoxy)phenyl)-2-(trimethylsilyloxy)acetonitrile

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Technology Process of 2-(4-methoxy-2-(methoxymethoxy)phenyl)-2-(trimethylsilyloxy)acetonitrile

There total 1 articles about 2-(4-methoxy-2-(methoxymethoxy)phenyl)-2-(trimethylsilyloxy)acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 7677-24-9
trimethylsilyl cyanide

: 124555-63-1
4-methoxy-2-methoxymethoxy benzaldehyde

: 1163251-97-5
2-(4-methoxy-2-(methoxymethoxy)phenyl)-2-(trimethylsilyloxy)acetonitrile

Guidance literature:: With potassium cyanide; 18-crown-6 ether; In benzene; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jo900648n

Reference yield: 21.0%

: 6,7-dimethoxy-3-nitro-chromene

: 1163251-97-5
2-(4-methoxy-2-(methoxymethoxy)phenyl)-2-(trimethylsilyloxy)acetonitrile

: 1163251-95-3
C₂₁H₂₂O₇

: cis-12a-hydroxymunduserone

Guidance literature:: 2-(4-methoxy-2-(methoxymethoxy)phenyl)-2-(trimethylsilyloxy)acetonitrile; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -70 ℃; for 0.25h; Inert atmosphere;

6,7-dimethoxy-3-nitro-chromene; In tetrahydrofuran; hexane; at -70 - 20 ℃; Further stages; Inert atmosphere;
DOI:10.1021/jo900648n

Reference yield: 10.0%

: 6,7-dimethoxy-3-nitro-chromene

: 1163251-97-5
2-(4-methoxy-2-(methoxymethoxy)phenyl)-2-(trimethylsilyloxy)acetonitrile

: 14630-04-7
2,3,9-trimethoxy-6H-chromeno[3,4-b]chromen-12-one

: 1163251-95-3
C₂₁H₂₂O₇

: cis-12a-hydroxymunduserone

Guidance literature:: 2-(4-methoxy-2-(methoxymethoxy)phenyl)-2-(trimethylsilyloxy)acetonitrile; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -70 ℃; for 0.25h; Inert atmosphere;

6,7-dimethoxy-3-nitro-chromene; In tetrahydrofuran; hexane; at -70 - 20 ℃; Further stages; Inert atmosphere;
DOI:10.1021/jo900648n