(S)-3-methylpentanoic acid ((1'S,2'S)-2'-hydroxy-1'-methyl-2'-phenylethyl)(methyl)amide

Base Information

Chemical Name:(S)-3-methylpentanoic acid ((1'S,2'S)-2'-hydroxy-1'-methyl-2'-phenylethyl)(methyl)amide
CAS No.:1122577-96-1
Molecular Formula:C₁₆H₂₅NO₂
Molecular Weight:263.38
Hs Code.:

Synonyms:(S)-3-methylpentanoic acid ((1'S,2'S)-2'-hydroxy-1'-methyl-2'-phenylethyl)(methyl)amide

Suppliers and Price of (S)-3-methylpentanoic acid ((1'S,2'S)-2'-hydroxy-1'-methyl-2'-phenylethyl)(methyl)amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-methylpentanoic acid ((1'S,2'S)-2'-hydroxy-1'-methyl-2'-phenylethyl)(methyl)amide

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Technology Process of (S)-3-methylpentanoic acid ((1'S,2'S)-2'-hydroxy-1'-methyl-2'-phenylethyl)(methyl)amide

There total 1 articles about (S)-3-methylpentanoic acid ((1'S,2'S)-2'-hydroxy-1'-methyl-2'-phenylethyl)(methyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1730-92-3
(3S)-methylvaleric acid

: 90-82-4,7009-81-6,90-83-5,6912-63-6
pseudoephedrine

: 1122577-96-1
(S)-3-methylpentanoic acid ((1'S,2'S)-2'-hydroxy-1'-methyl-2'-phenylethyl)(methyl)amide

Guidance literature:: (3S)-methylvaleric acid; With pivaloyl chloride; triethylamine; In dichloromethane; at -5 ℃; for 1h; Inert atmosphere;

pseudoephedrine; With triethylamine; In dichloromethane; at 5 ℃; Inert atmosphere;
DOI:10.1021/jm4007565

Reference yield: 92.0%

: 1122577-96-1
(S)-3-methylpentanoic acid ((1'S,2'S)-2'-hydroxy-1'-methyl-2'-phenylethyl)(methyl)amide

: 1730-92-3
(3S)-methylvaleric acid

Guidance literature:: With sulfuric acid; water; for 5h; Inert atmosphere; Heating;
DOI:10.1021/op800260j

Reference yield:

: 1122577-96-1
(S)-3-methylpentanoic acid ((1'S,2'S)-2'-hydroxy-1'-methyl-2'-phenylethyl)(methyl)amide

: 107-08-4
1-iodo-propane

: 1449396-57-9
C₁₉H₃₁NO₂

Guidance literature:: (S)-3-methylpentanoic acid ((1'S,2'S)-2'-hydroxy-1'-methyl-2'-phenylethyl)(methyl)amide; With n-butyllithium; diisopropylamine; lithium chloride; In tetrahydrofuran; cyclohexene; at -20 ℃; for 0.5h; Inert atmosphere;

1-iodo-propane; In tetrahydrofuran; cyclohexane; at -10 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jm4007565