(2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)prop-2-enoic acid

Base Information

Chemical Name:(2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)prop-2-enoic acid
CAS No.:1345471-52-4
Molecular Formula:C₂₀H₁₇F₅O₄
Molecular Weight:416.345
Hs Code.:

Synonyms:(2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)prop-2-enoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)prop-2-enoic acid

Chemical Property:

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Technology Process of (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)prop-2-enoic acid

There total 4 articles about (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)prop-2-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1345471-49-9
methyl (2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoate

: 1345471-52-4
(2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)prop-2-enoic acid

Guidance literature:: In 1,4-dioxane; water;

Reference yield:

: 921623-31-6
4-(4,4,4-trifluorobutoxy)benzoic acid

: 1345471-52-4
(2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)prop-2-enoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: trifluorormethanesulfonic acid

2: triethylamine; bromine; sodium hydrogencarbonate / dichloromethane; toluene; ethyl acetate

3: palladium diacetate / N,N-dimethyl-formamide

4: 1,4-dioxane; water

With trifluorormethanesulfonic acid; bromine; palladium diacetate; sodium hydrogencarbonate; triethylamine; In 1,4-dioxane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1345471-42-2
2-[4-(4,4,4-trifluorobutoxy)phenyl]-5,6-dihydro-4H-1,3-dithiin-1-ium trifluoromethanesulfonate

: 1345471-52-4
(2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)prop-2-enoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; bromine; sodium hydrogencarbonate / dichloromethane; toluene; ethyl acetate

2: palladium diacetate / N,N-dimethyl-formamide

3: 1,4-dioxane; water

With bromine; palladium diacetate; sodium hydrogencarbonate; triethylamine; In 1,4-dioxane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;