C₃₆H₃₄FNO₇SSe

Base Information

Chemical Name:C₃₆H₃₄FNO₇SSe
CAS No.:1374234-76-0
Molecular Formula:C₃₆H₃₄FNO₇SSe
Molecular Weight:722.693
Hs Code.:

C<sub>36</sub>H<sub>34</sub>FNO<sub>7</sub>SSe

Synonyms:C₃₆H₃₄FNO₇SSe

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Chemical Property of C₃₆H₃₄FNO₇SSe

Chemical Property:

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Technology Process of C₃₆H₃₄FNO₇SSe

There total 12 articles about C₃₆H₃₄FNO₇SSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 71098-88-9
N-phenylselanylphthalimide

: 1374234-75-9
C₃₀H₃₀FNO₇S

: 1374234-76-0
C₃₆H₃₄FNO₇SSe

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 26510-95-2
ethyl 4-Bromobenzoylacetate

: 1374234-76-0
C₃₆H₃₄FNO₇SSe

Guidance literature:: Multi-step reaction with 13 steps

1.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

2.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

2.2: 4 h / 80 °C

3.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

4.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

5.1: boron trichloride / dichloromethane / -78 - -40 °C

6.1: triethylamine / dmap / dichloromethane / 1 h / 0 - 20 °C

7.1: sodium acetate / (diphenylphosphin)ferrocene; palladium diacetate / acetonitrile / 2 h / 100 °C / Inert atmosphere

8.1: hydrogenchloride; water / tetrahydrofuran / 1 h / Reflux

9.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

9.2: 20 °C / pH 8 - 9

10.1: pyridine / 2 h / 0 - 30 °C

11.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

12.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 2 h / 0 °C

13.1: camphor-10-sulfonic acid / dichloromethane / 0 - 20 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; potassium phosphate; tin(II) chloride dihdyrate; camphor-10-sulfonic acid; water; nitric acid; sodium acetate; boron trichloride; potassium carbonate; caesium carbonate; triethylamine; zinc(II) chloride; dmap; (diphenylphosphin)ferrocene; palladium diacetate; tert-butyl XPhos; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 99-90-1
para-bromoacetophenone

: 1374234-76-0
C₃₆H₃₄FNO₇SSe

Guidance literature:: Multi-step reaction with 14 steps

1.1: sodium hydride / toluene; mineral oil / 2 h / 0 - 20 °C

1.2: Reflux

2.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

3.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

3.2: 4 h / 80 °C

4.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

5.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

6.1: boron trichloride / dichloromethane / -78 - -40 °C

7.1: triethylamine / dmap / dichloromethane / 1 h / 0 - 20 °C

8.1: sodium acetate / (diphenylphosphin)ferrocene; palladium diacetate / acetonitrile / 2 h / 100 °C / Inert atmosphere

9.1: hydrogenchloride; water / tetrahydrofuran / 1 h / Reflux

10.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

10.2: 20 °C / pH 8 - 9

11.1: pyridine / 2 h / 0 - 30 °C

12.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

13.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 2 h / 0 °C

14.1: camphor-10-sulfonic acid / dichloromethane / 0 - 20 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; potassium phosphate; tin(II) chloride dihdyrate; camphor-10-sulfonic acid; water; nitric acid; sodium acetate; boron trichloride; sodium hydride; potassium carbonate; caesium carbonate; triethylamine; zinc(II) chloride; dmap; (diphenylphosphin)ferrocene; palladium diacetate; tert-butyl XPhos; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil;