tris([(3-benzyloxy-4-oxo-4H-pyran-2-yl)carbonylamino]propyl)-nitromethane

Base Information

• Chemical Name: tris([(3-benzyloxy-4-oxo-4H-pyran-2-yl)carbonylamino]propyl)-nitromethane
• CAS No.: 1037293-77-8
• Molecular Formula: C₄₉H₄₈N₄O₁₄
• Molecular Weight: 916.939

Synonyms:tris([(3-benzyloxy-4-oxo-4H-pyran-2-yl)carbonylamino]propyl)-nitromethane

Chemical Property of tris([(3-benzyloxy-4-oxo-4H-pyran-2-yl)carbonylamino]propyl)-nitromethane

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Technology Process of tris([(3-benzyloxy-4-oxo-4H-pyran-2-yl)carbonylamino]propyl)-nitromethane

There total 1 articles about tris([(3-benzyloxy-4-oxo-4H-pyran-2-yl)carbonylamino]propyl)-nitromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

3-benzyloxy-4-oxo-4H-pyran-2-carboxylic acid 2,5-dioxo-pyrrolidin-1-yl ester (1037293-71-2) + 1,7-diamino-4-nitro-4-(3-amino-propyl)-heptane tris(trifluoroacetate) → tris([(3-benzyloxy-4-oxo-4H-pyran-2-yl)carbonylamino]propyl)-nitromethane (1037293-77-8)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield: 57.0%

tris([(3-benzyloxy-4-oxo-4H-pyran-2-yl)carbonylamino]propyl)-nitromethane (1037293-77-8) + 2-methoxyethylamine (109-85-3) → tris[2-(carboxyaminoprop-3-yl)-3-benzyloxy-1-(2-methoxyethyl)-4-oxo-1,4-dihydro-pyridine]nitro-methane (1037293-78-9)

Guidance literature:

In methanol; for 1h; Heating / reflux;

Reference yield: 45.0%

tris([(3-benzyloxy-4-oxo-4H-pyran-2-yl)carbonylamino]propyl)-nitromethane (1037293-77-8) + ethanolamine (141-43-5) → tris([3-benzyloxy-1-(2-hydroxyethyl)-4-oxo-4H-pyridin-2-ylcarbonylamino]prop-1-yl)nitromethane (1037294-02-2)

Guidance literature:

In methanol; for 1h; Heating / reflux;

upstream raw materials:

3-benzyloxy-4-oxo-4H-pyran-2-carboxylic acid 2,5-dioxo-pyrrolidin-1-yl ester

Downstream raw materials:

tris[2-(carboxyaminoprop-3-yl)-3-benzyloxy-1-(2-methoxyethyl)-4-oxo-1,4-dihydro-pyridine]nitro-methane

tris([3-benzyloxy-1-(2-hydroxyethyl)-4-oxo-4H-pyridin-2-ylcarbonylamino]prop-1-yl)nitromethane

tris((3-benzyloxy-1-(2,3,4,5,6-pentahydroxy-n-hexane)-4-oxo-4H-4-pyridone-2-yl)carboxyaminopropyl)nitromethane

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