Technology Process of 2-benzyloxy-4-nitrophenol
There total 4 articles about 2-benzyloxy-4-nitrophenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-(benzyloxy)-1-methoxy-4-nitrobenzene;
With
sodium hydroxide;
In
dimethyl sulfoxide;
at 95 ℃;
for 15h;
Industry scale;
With
hydrogenchloride;
In
water; dimethyl sulfoxide; toluene;
at 20 ℃;
pH=1;
With
potassium hydroxide;
In
isopropyl alcohol; toluene;
at 40 ℃;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / Inert atmosphere
1.2: 18 h / 70 °C
2.1: sodium hydroxide / dimethyl sulfoxide / 15 h / 95 °C / Industry scale
2.2: 20 °C / pH 1
2.3: 40 °C
With
potassium carbonate; sodium hydroxide;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrabutylammomium bromide; sodium hydroxide / water; toluene / 3 h / 50 - 55 °C / Inert atmosphere
2.1: sodium hydroxide / dimethyl sulfoxide / 15 h / 95 °C / Industry scale
2.2: 20 °C / pH 1
2.3: 40 °C
With
tetrabutylammomium bromide; sodium hydroxide;
In
water; dimethyl sulfoxide; toluene;
