2-benzyloxy-4-nitrophenol

Base Information

Chemical Name:2-benzyloxy-4-nitrophenol
CAS No.:1064662-78-7
Molecular Formula:C₁₃H₁₀NO₄*K
Molecular Weight:283.325
Hs Code.:

Synonyms:2-benzyloxy-4-nitrophenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzyloxy-4-nitrophenol

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Technology Process of 2-benzyloxy-4-nitrophenol

There total 4 articles about 2-benzyloxy-4-nitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 75167-86-1
2-(benzyloxy)-1-methoxy-4-nitrobenzene

: 1064662-78-7
2-benzyloxy-4-nitrophenol

Guidance literature:: 2-(benzyloxy)-1-methoxy-4-nitrobenzene; With sodium hydroxide; In dimethyl sulfoxide; at 95 ℃; for 15h; Industry scale;

With hydrogenchloride; In water; dimethyl sulfoxide; toluene; at 20 ℃; pH=1;

With potassium hydroxide; In isopropyl alcohol; toluene; at 40 ℃;

Reference yield:

: 636-93-1
5-nitroguaiacol

: 1064662-78-7
2-benzyloxy-4-nitrophenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / Inert atmosphere

1.2: 18 h / 70 °C

2.1: sodium hydroxide / dimethyl sulfoxide / 15 h / 95 °C / Industry scale

2.2: 20 °C / pH 1

2.3: 40 °C

With potassium carbonate; sodium hydroxide; In dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 100-39-0
benzyl bromide

: 1064662-78-7
2-benzyloxy-4-nitrophenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutylammomium bromide; sodium hydroxide / water; toluene / 3 h / 50 - 55 °C / Inert atmosphere

2.1: sodium hydroxide / dimethyl sulfoxide / 15 h / 95 °C / Industry scale

2.2: 20 °C / pH 1

2.3: 40 °C

With tetrabutylammomium bromide; sodium hydroxide; In water; dimethyl sulfoxide; toluene;