diethyl (γ-(N-(p-methoxybenzylidene)amino)propyl)acetamidomalonate N-oxide

Base Information

Chemical Name:diethyl (γ-(N-(p-methoxybenzylidene)amino)propyl)acetamidomalonate N-oxide
CAS No.:144811-53-0
Molecular Formula:C₂₀H₂₈N₂O₇
Molecular Weight:408.452
Hs Code.:

Synonyms:diethyl (γ-(N-(p-methoxybenzylidene)amino)propyl)acetamidomalonate N-oxide

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Chemical Property of diethyl (γ-(N-(p-methoxybenzylidene)amino)propyl)acetamidomalonate N-oxide

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Technology Process of diethyl (γ-(N-(p-methoxybenzylidene)amino)propyl)acetamidomalonate N-oxide

There total 4 articles about diethyl (γ-(N-(p-methoxybenzylidene)amino)propyl)acetamidomalonate N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 144811-53-0
diethyl (γ-(N-(p-methoxybenzylidene)amino)propyl)acetamidomalonate N-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / benzene / 4 h / 110 °C

2: monoperoxyphthalic acid magnesium salt / ethanol; diethyl ether / 3 h / 0 °C

3: silica gel

With silica gel; Monoperoxyphthalic acid, magnesium salt; triethylamine; In diethyl ether; ethanol; benzene;

Reference yield:

: 144811-54-1
2-Acetylamino-2-(3-amino-propyl)-malonic acid diethyl ester

: 144811-53-0
diethyl (γ-(N-(p-methoxybenzylidene)amino)propyl)acetamidomalonate N-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / benzene / 4 h / 110 °C

2: monoperoxyphthalic acid magnesium salt / ethanol; diethyl ether / 3 h / 0 °C

3: silica gel

With silica gel; Monoperoxyphthalic acid, magnesium salt; triethylamine; In diethyl ether; ethanol; benzene;

Reference yield:

: 2-Acetylamino-2-(3-{[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-amino}-propyl)-malonic acid diethyl ester

: 144811-53-0
diethyl (γ-(N-(p-methoxybenzylidene)amino)propyl)acetamidomalonate N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: monoperoxyphthalic acid magnesium salt / ethanol; diethyl ether / 3 h / 0 °C

2: silica gel

With silica gel; Monoperoxyphthalic acid, magnesium salt; In diethyl ether; ethanol;