1,6-bis-(4-ethoxy-phenyl)-hex-1-ene

Base Information

• Chemical Name: 1,6-bis-(4-ethoxy-phenyl)-hex-1-ene
• CAS No.: 102473-16-5
• Molecular Formula: C₂₂H₂₈O₂
• Molecular Weight: 324.463
• Mol file: 102473-16-5.mol

Synonyms:1,6-bis-(4-ethoxy-phenyl)-hex-1-ene

Chemical Property of 1,6-bis-(4-ethoxy-phenyl)-hex-1-ene

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of 1,6-bis-(4-ethoxy-phenyl)-hex-1-ene

There total 9 articles about 1,6-bis-(4-ethoxy-phenyl)-hex-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(4-ethoxy-phenyl)-5-oxo-valeric acid (34670-10-5) → 1,6-bis-(4-ethoxy-phenyl)-hex-1-ene (102473-16-5)

Guidance literature:

Multi-step reaction with 5 steps

1: amalgamated zinc; aqueous hydrochloric acid; ethanol / Erwaermen des Reaktionsprodukts mit wss.-aethanol. Natronlauge

2: ethanol; sulfuric acid

4: benzene; PBr₃

With hydrogenchloride; amalgamated zinc; ethanol; sulfuric acid; phosphorus tribromide; benzene;

DOI:10.1080/10789669.2002.10391436

Reference yield:

5-(4-ethoxy-phenyl)-valeric acid (749250-48-4) → 1,6-bis-(4-ethoxy-phenyl)-hex-1-ene (102473-16-5)

Guidance literature:

Multi-step reaction with 4 steps

1: ethanol; sulfuric acid

3: benzene; PBr₃

With ethanol; sulfuric acid; phosphorus tribromide; benzene;

DOI:10.1080/10789669.2002.10391436

Reference yield:

5-(4-ethoxy-phenyl)-valeric acid ethyl ester (854659-02-2) → 1,6-bis-(4-ethoxy-phenyl)-hex-1-ene (102473-16-5)

Guidance literature:

Multi-step reaction with 3 steps

2: benzene; PBr₃

With phosphorus tribromide; benzene;

DOI:10.1080/10789669.2002.10391436

upstream raw materials:

p-ethoxyallylbenzene

4-(5-bromo-pentyl)-phenetole

4-ethoxybenzaldehyde

diethyl ether

Downstream raw materials:

4-(ethoxy)benzoic acid

5-(4-ethoxy-phenyl)-valeric acid