trimethyl 12-oxo-8-phenyl-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

Base Information

Chemical Name:trimethyl 12-oxo-8-phenyl-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate
CAS No.:1315594-36-5
Molecular Formula:C₃₀H₂₀N₂O₇
Molecular Weight:520.498
Hs Code.:

Synonyms:trimethyl 12-oxo-8-phenyl-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

Suppliers and Price of trimethyl 12-oxo-8-phenyl-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trimethyl 12-oxo-8-phenyl-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trimethyl 12-oxo-8-phenyl-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

There total 2 articles about trimethyl 12-oxo-8-phenyl-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1315594-32-1
2-(1H-perimidin-2(3H)-ylidene)-1-phenylethan-1-one

: 762-42-5
dimethyl acetylenedicarboxylate

: 1315594-36-5
trimethyl 12-oxo-8-phenyl-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

Guidance literature:: With dmap; In ethyl acetate; for 0.5h; Reflux;
DOI:10.1016/j.tet.2011.05.078

Reference yield:

: 479-27-6
naphthalene-1,8-diamine

: 1315594-36-5
trimethyl 12-oxo-8-phenyl-12H-isoindolo[2,1-a]perimidine-9,10,11-tricarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 5 h / Reflux

2: dmap / ethyl acetate / 0.5 h / Reflux

With dmap; toluene-4-sulfonic acid; In 5,5-dimethyl-1,3-cyclohexadiene; ethyl acetate;
DOI:10.1016/j.tet.2011.05.078