trisodium 2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

Base Information

Chemical Name:trisodium 2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate
CAS No.:108786-35-2
Molecular Formula:C₃₉H₃₆N₃O₁₅*3Na
Molecular Weight:855.695
Hs Code.:

Synonyms:trisodium 2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trisodium 2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

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Technology Process of trisodium 2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

There total 5 articles about trisodium 2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60541-32-4
benzene-1,3,5-tricarboxamide

: 108786-35-2
trisodium 2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium boranate, borontrifluoride etherate, 2.) cc.HCl / 1.) THF, room temperature, 3 d, than reflux, 4 d, 2.) THF, reflux, 4 h

2: 95 percent / triethylamine / N,N-dimethyl-acetamide / 4 h

3: NaOH / methanol; H₂O

With hydrogenchloride; sodium hydroxide; sodium metaborate; boron trifluoride diethyl etherate; triethylamine; In methanol; N,N-dimethyl acetamide; water;
DOI:10.1016/S0040-4020(01)87606-7

Reference yield:

: 92078-26-7
trimethyl-2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

: 108786-35-2
trisodium 2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

Guidance literature:: With sodium hydroxide; In methanol; water; Yield given;
DOI:10.1016/S0040-4020(01)87606-7

Reference yield:

: 7168-94-7
dimethyl 2,3-dimethoxyterephthalate

: 108786-35-2
trisodium 2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / NaOH / methanol; H₂O / Heating

2: 90 percent / thionyl chloride / 0.5 h / Heating

3: 95 percent / triethylamine / N,N-dimethyl-acetamide / 4 h

4: NaOH / methanol; H₂O

With sodium hydroxide; thionyl chloride; triethylamine; In methanol; N,N-dimethyl acetamide; water;
DOI:10.1016/S0040-4020(01)87606-7