6-(3-hydroxymethyl-2,2,4-trimethyl-cyclohex-3-enyl)-6-(2-methoxy-ethoxymethoxy)-hex-4-en-1-ol

Base Information

Chemical Name:6-(3-hydroxymethyl-2,2,4-trimethyl-cyclohex-3-enyl)-6-(2-methoxy-ethoxymethoxy)-hex-4-en-1-ol
CAS No.:925212-42-6
Molecular Formula:C₂₀H₃₆O₅
Molecular Weight:356.503
Hs Code.:

Synonyms:6-(3-hydroxymethyl-2,2,4-trimethyl-cyclohex-3-enyl)-6-(2-methoxy-ethoxymethoxy)-hex-4-en-1-ol

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Chemical Property of 6-(3-hydroxymethyl-2,2,4-trimethyl-cyclohex-3-enyl)-6-(2-methoxy-ethoxymethoxy)-hex-4-en-1-ol

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Technology Process of 6-(3-hydroxymethyl-2,2,4-trimethyl-cyclohex-3-enyl)-6-(2-methoxy-ethoxymethoxy)-hex-4-en-1-ol

There total 5 articles about 6-(3-hydroxymethyl-2,2,4-trimethyl-cyclohex-3-enyl)-6-(2-methoxy-ethoxymethoxy)-hex-4-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 925212-69-7
acetic acid 5-[6-hydroxy-1-(2-methoxy-ethoxymethoxy)-hex-2-enyl]-2,6,6-trimethyl-cyclohex-1-enylmethyl ester

: 925212-42-6
6-(3-hydroxymethyl-2,2,4-trimethyl-cyclohex-3-enyl)-6-(2-methoxy-ethoxymethoxy)-hex-4-en-1-ol

Guidance literature:: With lithium hydroxide; In methanol; water; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2006.10.058

Reference yield:

: 925212-41-5
[5-((E)-6-[tert-butyldimethylsilyloxy]-1-hydroxy-2-hexenyl)-2,6,6-trimethyl-1-cyclohexenyl]methyl acetate

: 925212-42-6
6-(3-hydroxymethyl-2,2,4-trimethyl-cyclohex-3-enyl)-6-(2-methoxy-ethoxymethoxy)-hex-4-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / diisopropylethylamine; DMAP / CH₂Cl₂ / 14 h / 20 °C

2: 90 percent / TBAF / tetrahydrofuran / 1 h / 20 °C

3: 85 percent / LiOH*H₂O / H₂O; methanol / 1 h / 20 °C

With dmap; lithium hydroxide; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.tet.2006.10.058

Reference yield:

: 925212-68-6
acetic acid 5-[6-(tert-butyl-dimethyl-silanyloxy)-1-(2-methoxy-ethoxymethoxy)-hex-2-enyl]-2,6,6-trimethyl-cyclohex-1-enylmethyl ester

: 925212-42-6
6-(3-hydroxymethyl-2,2,4-trimethyl-cyclohex-3-enyl)-6-(2-methoxy-ethoxymethoxy)-hex-4-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / TBAF / tetrahydrofuran / 1 h / 20 °C

2: 85 percent / LiOH*H₂O / H₂O; methanol / 1 h / 20 °C

With lithium hydroxide; tetrabutyl ammonium fluoride; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.tet.2006.10.058