Technology Process of DL-1,2,3,4-Tetra-O-acetyl-6-O-benzyl-5-deoxy-5-fluoro-myo-inositol
There total 8 articles about DL-1,2,3,4-Tetra-O-acetyl-6-O-benzyl-5-deoxy-5-fluoro-myo-inositol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 96 percent / 5 M aq. NaOH / methanol / 4 h
2: diethylaminosulfur trifluoride / 4 h / -20 deg C to r.t.
3: 80 percent acetic acid / 3 h / Heating
4: pyridine / 3 h / 65 °C
With
pyridine; sodium hydroxide; diethylamino-sulfur trifluoride; acetic acid;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dimethylformamide / 12 h / 140 °C
2: 96 percent / 5 M aq. NaOH / methanol / 4 h
3: diethylaminosulfur trifluoride / 4 h / -20 deg C to r.t.
4: 80 percent acetic acid / 3 h / Heating
5: pyridine / 3 h / 65 °C
With
pyridine; sodium hydroxide; diethylamino-sulfur trifluoride; acetic acid;
In
methanol; N,N-dimethyl-formamide;
-
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40773-58-8,40773-59-9,81601-24-3,92217-61-3,92217-62-4,99147-11-2,114716-74-4,116907-54-1,117708-44-8,124601-98-5,129707-20-6
DL-6-O-Benzyl-1,2:3,4-di-O-cyclohexylidene-myo-inositol
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 95 percent / pyridine / 12 h / Ambient temperature
2: dimethylformamide / 12 h / 140 °C
3: 96 percent / 5 M aq. NaOH / methanol / 4 h
4: diethylaminosulfur trifluoride / 4 h / -20 deg C to r.t.
5: 80 percent acetic acid / 3 h / Heating
6: pyridine / 3 h / 65 °C
With
pyridine; sodium hydroxide; diethylamino-sulfur trifluoride; acetic acid;
In
methanol; N,N-dimethyl-formamide;
