C₆H₁₁PCl₃⁽¹⁺⁾*GaCl₄^(1-)=C₆H₁₁PCl₃GaCl₄

Base Information

Chemical Name:C₆H₁₁PCl₃⁽¹⁺⁾*GaCl₄^(1-)=C₆H₁₁PCl₃GaCl₄
CAS No.:1199269-74-3
Molecular Formula:C₆H₁₁Cl₃P*Cl₄Ga
Molecular Weight:432.021
Hs Code.:

C<sub>6</sub>H<sub>11</sub>PCl<sub>3</sub><sup>(1+)</sup>*GaCl<sub>4</sub><sup>(1-)</sup>=C<sub>6</sub>H<sub>11</sub>PCl<sub>3</sub>GaCl<sub>4</sub>

Synonyms:C₆H₁₁PCl₃⁽¹⁺⁾*GaCl₄^(1-)=C₆H₁₁PCl₃GaCl₄

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Chemical Property of C₆H₁₁PCl₃⁽¹⁺⁾*GaCl₄^(1-)=C₆H₁₁PCl₃GaCl₄

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Technology Process of C₆H₁₁PCl₃⁽¹⁺⁾*GaCl₄^(1-)=C₆H₁₁PCl₃GaCl₄

There total 2 articles about C₆H₁₁PCl₃⁽¹⁺⁾*GaCl₄^(1-)=C₆H₁₁PCl₃GaCl₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1,2,3,4-tetracyclohexyl-cyclo-2-chloro-1,3,4-triphosphino-2-phosphonium heptachlorodigallate

: 10026-13-8,874483-75-7
phosphorus pentachloride

: 1199269-74-3
C₆H₁₁PCl₃⁽¹⁺⁾*GaCl₄^(1-)=C₆H₁₁PCl₃GaCl₄

Guidance literature:: In dichloromethane; (N2) a soln. of PCl5 in CH2Cl2 was added dropwise to a stirred soln. of complex in CH2Cl2, the mixt. was stirred at room temp. for 5 h; the solvent was partially removed in vac., layered with pentane and stored at -32°C within two days;
DOI:10.1021/ja907693f

Reference yield: 74.0%

: 10026-13-8,874483-75-7
phosphorus pentachloride

: 13450-91-4
gallium(III) iodide

: 3040-71-9
tetracyclohexylcyclotetraphosphine

: 1199269-74-3
C₆H₁₁PCl₃⁽¹⁺⁾*GaCl₄^(1-)=C₆H₁₁PCl₃GaCl₄

Guidance literature:: In dichloromethane; (N2) to a soln. of (C6H11P)4 and GaCl3 in CH2Cl2 was slowly added a soln. of PCl5 in CH2Cl2 at room temp.; the solvent was partially removed in vac., layered with pentane and stored at -32°C within two days; elem. anal.;
DOI:10.1021/ja907693f