tris-(pentafluoro phenyl) germane thiol

Base Information

Chemical Name:tris-(pentafluoro phenyl) germane thiol
CAS No.:54666-68-1
Molecular Formula:C₁₈HF₁₅GeS
Molecular Weight:606.838
Hs Code.:

Synonyms:tris-(pentafluoro phenyl) germane thiol

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Chemical Property of tris-(pentafluoro phenyl) germane thiol

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Technology Process of tris-(pentafluoro phenyl) germane thiol

There total 3 articles about tris-(pentafluoro phenyl) germane thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: ((C₆F₅)3Ge)2HgSGe(C₆F₅)3^(1-)*(C₅H₅)2Co⁽¹⁺⁾=((C₆F₅)3Ge)2HgSGe(C₆F₅)3((C₅H₅)2Co)

: 54666-68-1
tris-(pentafluoro phenyl) germane thiol

: 35406-49-6
bis[tris(pentafluorophenyl)germyl]mercury

: 7783-06-4
hydrogen sulfide

: 42371-50-6
tris(pentafuorophenyl)germane

: 1259-89-8
Chloro[tris(perfluorophenyl)]-germane

Guidance literature:: With hydrogen chloride; In tetrahydrofuran; byproducts: Cp2CoCl; HCl was added to a THF soln. of monothiomercurate, mixt. was kept in a sealed ampoule at 20°C for 1 h; solvent and volatiles (H2S) were removed, residue was extd. with hexane, ext. contained Ar3GeH, Ar3GeCl, and Ar3GeSH (GLC and LSC analyses), residue contained (Ar3Ge)2Hg and cobalt-containing product, probably Cp2CoCl (IR spectral and LSC data);
DOI:10.1016/S0022-328X(00)99406-3

Reference yield: 76.8%

: 7610-18-6
triethyl germane thiol

: 10360-39-1
tris(pentafluorophenyl)germanium bromide

: 54666-68-1
tris-(pentafluoro phenyl) germane thiol

Guidance literature:: In neat (no solvent); heating at 150°C, 18 hours;;
DOI:10.1016/S0022-328X(00)80720-2

Reference yield: 58.0%

: 42371-50-6
tris(pentafuorophenyl)germane

: 7704-34-9
sulfur

: 54666-68-1
tris-(pentafluoro phenyl) germane thiol

Guidance literature:: In neat (no solvent); heating at 135°C, 2 hours, then at 150°C, 1.5 hours;; recrystallization from hexane;;
DOI:10.1016/S0022-328X(00)80720-2