N-<3-(5-methyl-2-methoxycarbonylphenoxy)propyl>-m-hydroxyphenylacetamide

Base Information

Chemical Name:N-<3-(5-methyl-2-methoxycarbonylphenoxy)propyl>-m-hydroxyphenylacetamide
CAS No.:115149-59-2
Molecular Formula:C₂₀H₂₃NO₅
Molecular Weight:357.406
Hs Code.:

Synonyms:N-<3-(5-methyl-2-methoxycarbonylphenoxy)propyl>-m-hydroxyphenylacetamide

Suppliers and Price of N-<3-(5-methyl-2-methoxycarbonylphenoxy)propyl>-m-hydroxyphenylacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-<3-(5-methyl-2-methoxycarbonylphenoxy)propyl>-m-hydroxyphenylacetamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-<3-(5-methyl-2-methoxycarbonylphenoxy)propyl>-m-hydroxyphenylacetamide

There total 4 articles about N-<3-(5-methyl-2-methoxycarbonylphenoxy)propyl>-m-hydroxyphenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 621-37-4
m-hydroxyphenylacetic acid

: 115149-56-9
methyl 2-(3-aminopropoxy)-4-methylbenzoate hydrochloride

: 115149-59-2
N-<3-(5-methyl-2-methoxycarbonylphenoxy)propyl>-m-hydroxyphenylacetamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; acetonitrile; for 24h; Ambient temperature;

Reference yield:

: 4670-56-8
methyl 2-hydroxy-4-methylbenzoate

: 115149-59-2
N-<3-(5-methyl-2-methoxycarbonylphenoxy)propyl>-m-hydroxyphenylacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / potassium carbonate / acetone / 24 h / Heating

2: 75 percent / conc. HCl / dioxane / 48 h / Heating

3: 81 percent / thionyl chloride / 0 deg C, 60 deg C, 10 h

4: 70 percent / Et₃N, 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochoride / acetonitrile; tetrahydrofuran / 24 h / Ambient temperature

With hydrogenchloride; thionyl chloride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; acetone; acetonitrile;

Reference yield:

: 115149-48-9
methyl 4-methyl-2-<3-(N-phthalimido)propoxy>benzoate

: 115149-59-2
N-<3-(5-methyl-2-methoxycarbonylphenoxy)propyl>-m-hydroxyphenylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / conc. HCl / dioxane / 48 h / Heating

2: 81 percent / thionyl chloride / 0 deg C, 60 deg C, 10 h

3: 70 percent / Et₃N, 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochoride / acetonitrile; tetrahydrofuran / 24 h / Ambient temperature

With hydrogenchloride; thionyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; acetonitrile;