3,6-di-O-acetyl-1,5-anhydro-4-O-benzoyl-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-glucitol

Base Information

Chemical Name:3,6-di-O-acetyl-1,5-anhydro-4-O-benzoyl-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-glucitol
CAS No.:502493-93-8
Molecular Formula:C₂₆H₂₉NO₉
Molecular Weight:499.518
Hs Code.:

Synonyms:3,6-di-O-acetyl-1,5-anhydro-4-O-benzoyl-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-glucitol

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Chemical Property of 3,6-di-O-acetyl-1,5-anhydro-4-O-benzoyl-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-glucitol

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Technology Process of 3,6-di-O-acetyl-1,5-anhydro-4-O-benzoyl-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-glucitol

There total 1 articles about 3,6-di-O-acetyl-1,5-anhydro-4-O-benzoyl-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: Benzoic acid (2R,3S,4R,5S)-4-acetoxy-2-acetoxymethyl-5-carboxymethyl-tetrahydro-pyran-3-yl ester

: 502493-93-8
3,6-di-O-acetyl-1,5-anhydro-4-O-benzoyl-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-glucitol

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/ol027458l

Reference yield:

: 502493-93-8
3,6-di-O-acetyl-1,5-anhydro-4-O-benzoyl-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-glucitol

: N-Benzyloxy-2-((3S,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-acetamide

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 3h; neutralized using Amberlite IR-120 (H⁽¹⁺⁾);
DOI:10.1021/ol027458l

Reference yield:

: 502493-93-8
3,6-di-O-acetyl-1,5-anhydro-4-O-benzoyl-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-glucitol

: 502493-94-9
1,5-anhydro-4,6-O-benzylidene-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-qlucitol

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / methanol / 3 h / 20 °C / neutralized using Amberlite IR-120 (H⁽¹⁺⁾)

2: TsOH*H₂O / acetonitrile / 3 h / 20 °C

With sodium methylate; toluene-4-sulfonic acid; In methanol; acetonitrile;
DOI:10.1021/ol027458l