1,5-anhydro-4,6-O-benzylidene-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-qlucitol

Base Information

Chemical Name:1,5-anhydro-4,6-O-benzylidene-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-qlucitol
CAS No.:502493-94-9
Molecular Formula:C₂₂H₂₅NO₆
Molecular Weight:399.444
Hs Code.:

Synonyms:1,5-anhydro-4,6-O-benzylidene-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-qlucitol

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Chemical Property of 1,5-anhydro-4,6-O-benzylidene-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-qlucitol

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Technology Process of 1,5-anhydro-4,6-O-benzylidene-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-qlucitol

There total 6 articles about 1,5-anhydro-4,6-O-benzylidene-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-qlucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 866865-78-3
Benzoic acid (2R,4aR,7S,8R,8aS)-7-(benzyloxycarbamoyl-methyl)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

: 502493-94-9
1,5-anhydro-4,6-O-benzylidene-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-qlucitol

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1016/j.carres.2011.02.004

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: N-Benzyloxy-2-((3S,4R,5S,6R)-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-acetamide

: 502493-94-9
1,5-anhydro-4,6-O-benzylidene-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-qlucitol

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1021/ol027458l

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 502493-94-9
1,5-anhydro-4,6-O-benzylidene-2-C-(carboxymethyl N-benzyloxyamide)-2-deoxy-D-qlucitol

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / EDAC*HCl; Et₃N / CH₂Cl₂ / 3 h / 20 °C

2: NaOMe / methanol / 3 h / 20 °C / neutralized using Amberlite IR-120 (H⁽¹⁺⁾)

3: TsOH*H₂O / acetonitrile / 3 h / 20 °C

With sodium methylate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/ol027458l