C₄₈H₃₃N₃

Base Information

Chemical Name:C₄₈H₃₃N₃
CAS No.:1285719-50-7
Molecular Formula:C₄₈H₃₃N₃
Molecular Weight:651.81
Hs Code.:

C<sub>48</sub>H<sub>33</sub>N<sub>3</sub>

Synonyms:C₄₈H₃₃N₃

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Chemical Property of C₄₈H₃₃N₃

Chemical Property:

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Technology Process of C₄₈H₃₃N₃

There total 4 articles about C₄₈H₃₃N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1028647-93-9
3-(4-bromophenyl)-9-phenyl-9H-carbazole

: 212385-73-4
9-(4’-bromo-[1,1‘-biphenyl]-4-yl)-9H-carbazole

: 1285719-50-7
C₄₈H₃₃N₃

Guidance literature:: 3-(4-bromophenyl)-9-phenyl-9H-carbazole; 9-(4’-bromo-[1,1‘-biphenyl]-4-yl)-9H-carbazole; With acetamide; copper(l) iodide; potassium carbonate; In ortho-diethylbenzene; at 175 ℃; for 38h; Inert atmosphere;

With water; potassium hydroxide; In ortho-diethylbenzene; at 175 ℃; for 5h;

Reference yield:

: 1150-62-5
N-phenylcarbazole

: 1285719-50-7
C₄₈H₃₃N₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium iodide; sulfuric acid; potassium iodate / ethanol / 2 h / 75 °C

2.1: n-butyllithium / toluene; hexane; diethyl ether / 1 h / -45 - -5 °C / Inert atmosphere

2.2: 2 h / -45 °C / Inert atmosphere

2.3: 20 °C / Inert atmosphere

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 10 h / Inert atmosphere; Reflux

4.1: potassium carbonate; copper(l) iodide; acetamide / ortho-diethylbenzene / 38 h / 175 °C / Inert atmosphere

4.2: 5 h / 175 °C

With acetamide; potassium iodate; copper(l) iodide; n-butyllithium; sulfuric acid; sodium carbonate; potassium carbonate; potassium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; ethanol; hexane; ortho-diethylbenzene; water; toluene;

Reference yield:

: 502161-03-7
3-iodo-9-phenyl-9H-carbazole

: 1285719-50-7
C₄₈H₃₃N₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / toluene; hexane; diethyl ether / 1 h / -45 - -5 °C / Inert atmosphere

1.2: 2 h / -45 °C / Inert atmosphere

1.3: 20 °C / Inert atmosphere

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 10 h / Inert atmosphere; Reflux

3.1: potassium carbonate; copper(l) iodide; acetamide / ortho-diethylbenzene / 38 h / 175 °C / Inert atmosphere

3.2: 5 h / 175 °C

With acetamide; copper(l) iodide; n-butyllithium; sodium carbonate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; hexane; ortho-diethylbenzene; water; toluene;