tert-butyl (S)-(2-(4-(allyloxy)phenyl)-1-(1H-tetrazol-5-yl)ethyl)carbamate

Base Information

Chemical Name:tert-butyl (S)-(2-(4-(allyloxy)phenyl)-1-(1H-tetrazol-5-yl)ethyl)carbamate
CAS No.:1609554-82-6
Molecular Formula:C₁₇H₂₃N₅O₃
Molecular Weight:345.401
Hs Code.:

Synonyms:tert-butyl (S)-(2-(4-(allyloxy)phenyl)-1-(1H-tetrazol-5-yl)ethyl)carbamate

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Chemical Property of tert-butyl (S)-(2-(4-(allyloxy)phenyl)-1-(1H-tetrazol-5-yl)ethyl)carbamate

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Technology Process of tert-butyl (S)-(2-(4-(allyloxy)phenyl)-1-(1H-tetrazol-5-yl)ethyl)carbamate

There total 3 articles about tert-butyl (S)-(2-(4-(allyloxy)phenyl)-1-(1H-tetrazol-5-yl)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609554-81-5
tert-butyl (S)-(2-(4-(allyloxy)phenyl)-1-cyanoethyl)carbamate

: 1609554-82-6
tert-butyl (S)-(2-(4-(allyloxy)phenyl)-1-(1H-tetrazol-5-yl)ethyl)carbamate

Guidance literature:: With sodium azide; acetic acid; triethylamine; In toluene; at 100 ℃; for 14h; Inert atmosphere;

Reference yield:

: 127132-38-1
N-(tert-butyloxycarbonyl)-O-allyl-(S)-tyrosine

: 1609554-82-6
tert-butyl (S)-(2-(4-(allyloxy)phenyl)-1-(1H-tetrazol-5-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloroformic acid ethyl ester; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.5 h / -10 °C / Inert atmosphere

1.2: 1.5 h / -10 - 20 °C / Inert atmosphere

2.1: Burgess Reagent / tetrahydrofuran; dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3.1: acetic acid; sodium azide; triethylamine / toluene / 14 h / 100 °C / Inert atmosphere

With sodium azide; Burgess Reagent; chloroformic acid ethyl ester; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 147363-12-0
tert-butyl (S)-(3-(4-(allyloxy)phenyl)-1-amino-1-oxopropan-2-yl)carbamate

: 1609554-82-6
tert-butyl (S)-(2-(4-(allyloxy)phenyl)-1-(1H-tetrazol-5-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: Burgess Reagent / tetrahydrofuran; dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2: acetic acid; sodium azide; triethylamine / toluene / 14 h / 100 °C / Inert atmosphere

With sodium azide; Burgess Reagent; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; toluene;