i-propyl 4-(4-benzyloxy-2-hydroxy-3,6-dimethylbenzoyloxy)-2-hydroxy-3,6-dimethylbenzoate

Base Information

Chemical Name:i-propyl 4-(4-benzyloxy-2-hydroxy-3,6-dimethylbenzoyloxy)-2-hydroxy-3,6-dimethylbenzoate
CAS No.:261174-61-2
Molecular Formula:C₂₈H₃₀O₇
Molecular Weight:478.542
Hs Code.:

Synonyms:i-propyl 4-(4-benzyloxy-2-hydroxy-3,6-dimethylbenzoyloxy)-2-hydroxy-3,6-dimethylbenzoate

Suppliers and Price of i-propyl 4-(4-benzyloxy-2-hydroxy-3,6-dimethylbenzoyloxy)-2-hydroxy-3,6-dimethylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of i-propyl 4-(4-benzyloxy-2-hydroxy-3,6-dimethylbenzoyloxy)-2-hydroxy-3,6-dimethylbenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of i-propyl 4-(4-benzyloxy-2-hydroxy-3,6-dimethylbenzoyloxy)-2-hydroxy-3,6-dimethylbenzoate

There total 4 articles about i-propyl 4-(4-benzyloxy-2-hydroxy-3,6-dimethylbenzoyloxy)-2-hydroxy-3,6-dimethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 56410-32-3
4-benzyloxy-2-hydroxy-3,6-dimethylbenzoic acid

: 261174-50-9
2,4-dihydroxy-3,6-dimethyl-benzoic acid isopropyl ester

: 261174-61-2
i-propyl 4-(4-benzyloxy-2-hydroxy-3,6-dimethylbenzoyloxy)-2-hydroxy-3,6-dimethylbenzoate

Guidance literature:: With trifluoroacetic anhydride; In toluene; at 20 ℃;
DOI:10.1016/S0223-5234(99)00132-4

Reference yield:

: 31581-32-5
ethyl 2,4-dihydroxy-3,6-dimethylbenzoate

: 261174-61-2
i-propyl 4-(4-benzyloxy-2-hydroxy-3,6-dimethylbenzoyloxy)-2-hydroxy-3,6-dimethylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / K₂CO₃ / acetone / 24 h / Heating

2: 84 percent / aq. KOH / dimethylsulfoxide / Heating

3: 65 percent / (CF₃-CO)2O / toluene / 20 °C

With potassium hydroxide; potassium carbonate; trifluoroacetic anhydride; In dimethyl sulfoxide; acetone; toluene; 1: Alkylation / 2: Hydrolysis / 3: Esterification;
DOI:10.1016/S0223-5234(99)00132-4

Reference yield:

: 56410-31-2
ethyl 4-benzyloxy-2-hydroxy-3,6-dimethylbenzoate

: 261174-61-2
i-propyl 4-(4-benzyloxy-2-hydroxy-3,6-dimethylbenzoyloxy)-2-hydroxy-3,6-dimethylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / aq. KOH / dimethylsulfoxide / Heating

2: 65 percent / (CF₃-CO)2O / toluene / 20 °C

With potassium hydroxide; trifluoroacetic anhydride; In dimethyl sulfoxide; toluene; 1: Hydrolysis / 2: Esterification;
DOI:10.1016/S0223-5234(99)00132-4