phenyl-2 butyrate de p-nitrophenyle

Base Information

Chemical Name:phenyl-2 butyrate de p-nitrophenyle
CAS No.:72289-61-3
Molecular Formula:C₁₆H₁₅NO₄
Molecular Weight:285.299
Hs Code.:

Synonyms:phenyl-2 butyrate de p-nitrophenyle

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Chemical Property of phenyl-2 butyrate de p-nitrophenyle

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Technology Process of phenyl-2 butyrate de p-nitrophenyle

There total 14 articles about phenyl-2 butyrate de p-nitrophenyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.8%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 90-27-7
2-Phenylbutyric acid

: 72289-61-3
phenyl-2 butyrate de p-nitrophenyle

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dimethyl sulfoxide; at 20 ℃; for 8h;
DOI:10.1016/j.molcatb.2011.07.010

Reference yield: 65.0%

: 90-27-7
2-Phenylbutyric acid

: 7693-46-1
4-Nitrophenyl chloroformate

: 72289-61-3
phenyl-2 butyrate de p-nitrophenyle

Guidance literature:: 2-Phenylbutyric acid; With triethylamine; In dichloromethane; for 0.166667h; Inert atmosphere;

4-Nitrophenyl chloroformate; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1039/c4cc09003a

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 72289-61-3
phenyl-2 butyrate de p-nitrophenyle

Guidance literature:: Multi-step reaction with 21 steps

1: dmap; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 8 h / 20 °C

2: Candida antarctica lipase B / dimethyl sulfoxide / 0.05 h / 30 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

3: dmap; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 8 h / 20 °C

4: Candida antarctica lipase B / dimethyl sulfoxide / 0.05 h / 30 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

5: dmap; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 8 h / 20 °C

6: Bacillus subtilis 168 SrfAD esterase / dimethyl sulfoxide / 0.05 h / 30 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

7: dmap; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 8 h / 20 °C

8: Candida antarctica lipase B / dimethyl sulfoxide / 0.05 h / 30 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

9: dmap; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 8 h / 20 °C

10: Candida antarctica lipase B / dimethyl sulfoxide / 0.05 h / 30 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

11: dmap; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 8 h / 20 °C

12: Candida antarctica lipase B / dimethyl sulfoxide / 0.05 h / 30 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

13: dmap; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 8 h / 20 °C

14: Bacillus subtilis 168 SrfAD esterase / dimethyl sulfoxide / 0.05 h / 30 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

15: dmap; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 8 h / 20 °C

16: Bacillus subtilis 168 SrfAD esterase / dimethyl sulfoxide / 0.05 h / 30 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

17: dmap; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 8 h / 20 °C

18: Bacillus subtilis 168 SrfAD esterase / dimethyl sulfoxide / 0.05 h / 30 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

19: dmap; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 8 h / 20 °C

20: Bacillus subtilis 168 SrfAD esterase / dimethyl sulfoxide / 0.05 h / 30 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

21: dmap; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 8 h / 20 °C

With dmap; Candida antarctica lipase B; Bacillus subtilis 168 SrfAD esterase; dicyclohexyl-carbodiimide; In dimethyl sulfoxide;
DOI:10.1016/j.molcatb.2011.07.010