4-(4'-chlorophenyl)-1-[1-carbonylmethyl-(2-methyl-1H-benzimidazole)]-thiosemicarbazide

Base Information

Chemical Name:4-(4'-chlorophenyl)-1-[1-carbonylmethyl-(2-methyl-1H-benzimidazole)]-thiosemicarbazide
CAS No.:343977-50-4
Molecular Formula:C₁₇H₁₆ClN₅OS
Molecular Weight:373.866
Hs Code.:

Synonyms:4-(4'-chlorophenyl)-1-[1-carbonylmethyl-(2-methyl-1H-benzimidazole)]-thiosemicarbazide

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Chemical Property of 4-(4'-chlorophenyl)-1-[1-carbonylmethyl-(2-methyl-1H-benzimidazole)]-thiosemicarbazide

Chemical Property:

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Technology Process of 4-(4'-chlorophenyl)-1-[1-carbonylmethyl-(2-methyl-1H-benzimidazole)]-thiosemicarbazide

There total 3 articles about 4-(4'-chlorophenyl)-1-[1-carbonylmethyl-(2-methyl-1H-benzimidazole)]-thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2131-55-7
4-Chlorophenyl isothiocyanate

: 97420-40-1
2-(2-methyl-1H-benzimidazol-1-yl)acetohydrazide

: 343977-50-4
4-(4'-chlorophenyl)-1-[1-carbonylmethyl-(2-methyl-1H-benzimidazole)]-thiosemicarbazide

Guidance literature:: In ethanol; for 3h; Heating;

Reference yield:

: 615-15-6
2-Methyl-1H-benzimidazole

: 343977-50-4
4-(4'-chlorophenyl)-1-[1-carbonylmethyl-(2-methyl-1H-benzimidazole)]-thiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / polyethylene glycol-4000; K₂CO₃ / acetone / 20 °C

2: 94 percent / 98 percent hydrazine hydrate / methanol / 3 h / Heating

3: 93 percent / ethanol / 3 h / Heating

With polyethylene glycol-4000; potassium carbonate; hydrazine hydrate; In methanol; ethanol; acetone;

Reference yield:

: 97420-36-5
ethyl 2-(2-methyl-1H-benzo[d]imidazol-1-yl)acetate

: 343977-50-4
4-(4'-chlorophenyl)-1-[1-carbonylmethyl-(2-methyl-1H-benzimidazole)]-thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / 98 percent hydrazine hydrate / methanol / 3 h / Heating

2: 93 percent / ethanol / 3 h / Heating

With hydrazine hydrate; In methanol; ethanol;